Technology Process of C20H18N2O5
There total 5 articles about C20H18N2O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(l) iodide; potassium carbonate;
In
dimethyl sulfoxide;
at 20 ℃;
for 2h;
DOI:10.1039/c2cc37070k
- Guidance literature:
-
Multi-step reaction with 3 steps
1: thionyl chloride / 3 h / 0 - 75 °C
2: N-ethyl-N,N-diisopropylamine / dichloromethane / 1.5 h / 0 - 20 °C / Inert atmosphere
3: copper(l) iodide; potassium carbonate / dimethyl sulfoxide / 2 h / 20 °C
With
copper(l) iodide; thionyl chloride; potassium carbonate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; dimethyl sulfoxide;
DOI:10.1039/c2cc37070k
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1.5 h / 0 - 20 °C / Inert atmosphere
2: copper(l) iodide; potassium carbonate / dimethyl sulfoxide / 2 h / 20 °C
With
copper(l) iodide; potassium carbonate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; dimethyl sulfoxide;
DOI:10.1039/c2cc37070k