N,N′-diisopropyl-1,1-diphenylphosphanecarboximidamide

Base Information

• Chemical Name: N,N′-diisopropyl-1,1-diphenylphosphanecarboximidamide
• CAS No.: 790655-23-1
• Molecular Formula: C₁₉H₂₅N₂P
• Molecular Weight: 312.395
• Mol file: 790655-23-1.mol

Synonyms:

Chemical Property of N,N′-diisopropyl-1,1-diphenylphosphanecarboximidamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N′-diisopropyl-1,1-diphenylphosphanecarboximidamide

There total 3 articles about N,N′-diisopropyl-1,1-diphenylphosphanecarboximidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

diphenylphosphane (829-85-6) + diisopropyl-carbodiimide (693-13-0) → N,N′-diisopropyl-1,1-diphenylphosphanecarboximidamide (790655-23-1,642494-33-5)

Guidance literature:

With C₃₄H₅₈N₇Si₄Y; In tetrahydrofuran; at 20 ℃; for 0.5h; Solvent; Reagent/catalyst; Inert atmosphere; Glovebox; Schlenk technique;

DOI:10.1021/acs.organomet.5b00628

Reference yield: 97.0%

diphenylphosphane (829-85-6) + diisopropyl-carbodiimide (693-13-0) → N,N′-diisopropyl-1,1-diphenylphosphanecarboximidamide (790655-23-1,642494-33-5) + tetramethylsilane (75-76-3)

Guidance literature:

With C₃₅H₆₆Si₃Y^(1-)*C₁₄H₃₀LiO₄⁽¹⁺⁾; In tetrahydrofuran; at 80 ℃; for 1h; Reagent/catalyst; Solvent; Temperature; Mechanism; Schlenk technique; Inert atmosphere;

DOI:10.1039/c5nj01136a

Reference yield:

diphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phosphine + diisopropyl-carbodiimide (693-13-0) → N,N′-diisopropyl-1,1-diphenylphosphanecarboximidamide (790655-23-1,642494-33-5)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene / 18 h / 20 °C

2: methanol / 0.5 h

In methanol; toluene;

DOI:10.1039/c7dt02305g

upstream raw materials:

diphenylphosphane

diisopropyl-carbodiimide

Downstream raw materials:

C₅₀H₅₆N₆PY

CuBr[(Ph₂PC(NiPr)2)AlMe₂]

Zr(N,N'-diisopropyl-P-diphenylphosphaguanidinate)(dimethylamido)3

PtMe₂(Ph₂PC(NiPr)NHiPr)2*toluene