Technology Process of 4-methyl-1,3-phenylene bis-[4-(4-n-tetradecylphenoxy)carbonyl benzoate]
There total 7 articles about 4-methyl-1,3-phenylene bis-[4-(4-n-tetradecylphenoxy)carbonyl benzoate] which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 24 h
2: recorcinol; sodium chlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol / 20 °C
3: thionyl chloride; N,N-dimethyl-formamide / 1 h / Reflux
4: triethylamine; pyridine / dichloromethane / 6 h / Inert atmosphere; Reflux
With
pyridine; dmap; sodium chlorite; sodium dihydrogenphosphate; thionyl chloride; triethylamine; N,N-dimethyl-formamide; dicyclohexyl-carbodiimide; recorcinol;
In
dichloromethane; water; tert-butyl alcohol;
DOI:10.1039/c4tc00533c
- Guidance literature:
-
Multi-step reaction with 3 steps
1: recorcinol; sodium chlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol / 20 °C
2: thionyl chloride; N,N-dimethyl-formamide / 1 h / Reflux
3: triethylamine; pyridine / dichloromethane / 6 h / Inert atmosphere; Reflux
With
pyridine; sodium chlorite; sodium dihydrogenphosphate; thionyl chloride; triethylamine; N,N-dimethyl-formamide; recorcinol;
In
dichloromethane; water; tert-butyl alcohol;
DOI:10.1039/c4tc00533c
- Guidance literature:
-
Multi-step reaction with 2 steps
1: thionyl chloride; N,N-dimethyl-formamide / 1 h / Reflux
2: triethylamine; pyridine / dichloromethane / 6 h / Inert atmosphere; Reflux
With
pyridine; thionyl chloride; triethylamine; N,N-dimethyl-formamide;
In
dichloromethane;
DOI:10.1039/c4tc00533c
