4-benzyl-5-methylpyridazine

Base Information

Chemical Name:4-benzyl-5-methylpyridazine
CAS No.:96753-46-7
Molecular Formula:C₁₂H₁₂N₂
Molecular Weight:184.241
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-benzyl-5-methylpyridazine

Chemical Property:

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Technology Process of 4-benzyl-5-methylpyridazine

There total 6 articles about 4-benzyl-5-methylpyridazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

: 96780-97-1
(5-methyl-4-pyridazinyl)phenylmethanol

: 96753-46-7
4-benzyl-5-methylpyridazine

: 96780-96-0
(5-methyl-4-pyridazinyl)phenylmethanone

Guidance literature:: With 2-(N,N-dimethylamino)ethanol; toluene-4-sulfonic acid; at 150 ℃; for 2.5h; under 0.008 Torr; Product distribution;

Reference yield:

: 53074-23-0
4-Benzoylpyridazine

: 96753-46-7
4-benzyl-5-methylpyridazine

Guidance literature:: Multi-step reaction with 4 steps

1: 4 percent / tetrahydrofuran; diethyl ether / 1)-78 deg C, 10 min 2)warm to room temp.

2: 98 percent / Br₂ / acetic acid / 0.5 h

3: 89 percent / NaBH₄ / methanol / Ambient temperature

4: 8 percent / p-toluenesulfonic acid/2-dimethylaminoethanol / 2.5 h / 180 °C / 0.01 Torr

With sodium tetrahydroborate; 2-(N,N-dimethylamino)ethanol; bromine; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; diethyl ether; acetic acid;

Reference yield:

: 1120-88-3
4-methylpyridazine

: 96753-46-7
4-benzyl-5-methylpyridazine

Guidance literature:: Multi-step reaction with 3 steps

1: 27 percent / di-t-butylperoxide, t-butylhydroperoxide, ferrosulfate heptahydrate, H₂SO₄ / acetic acid / 1 h / 0 °C

2: 89 percent / NaBH₄ / methanol / Ambient temperature

3: 8 percent / p-toluenesulfonic acid/2-dimethylaminoethanol / 2.5 h / 180 °C / 0.01 Torr

With tert.-butylhydroperoxide; sodium tetrahydroborate; 2-(N,N-dimethylamino)ethanol; di-tert-butyl peroxide; sulfuric acid; toluene-4-sulfonic acid; iron(II) sulfate; In methanol; acetic acid;