4-Hydroxy-1-(4-(3-(1H-imidazol-4-yl)propyloxy)phenyl)butanone ethylene acetal

Base Information

Chemical Name:4-Hydroxy-1-(4-(3-(1H-imidazol-4-yl)propyloxy)phenyl)butanone ethylene acetal
CAS No.:184027-48-3
Molecular Formula:C₁₈H₂₄N₂O₄
Molecular Weight:332.4
Hs Code.:

Synonyms:

Suppliers and Price of 4-Hydroxy-1-(4-(3-(1H-imidazol-4-yl)propyloxy)phenyl)butanone ethylene acetal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Hydroxy-1-(4-(3-(1H-imidazol-4-yl)propyloxy)phenyl)butanone ethylene acetal

Chemical Property:

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Technology Process of 4-Hydroxy-1-(4-(3-(1H-imidazol-4-yl)propyloxy)phenyl)butanone ethylene acetal

There total 6 articles about 4-Hydroxy-1-(4-(3-(1H-imidazol-4-yl)propyloxy)phenyl)butanone ethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 152030-49-4
3-(1-trityl-1H-imidazol-4-yl)propan-1-ol

: 184027-48-3
4-Hydroxy-1-(4-(3-(1H-imidazol-4-yl)propyloxy)phenyl)butanone ethylene acetal

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / toluene

1.2: toluene / Heating

2.1: aq. HCl / tetrahydrofuran / Heating

3.1: p-TsOH / Heating

With hydrogenchloride; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; toluene; 1.1: Metallation / 1.2: Etherification / 2.1: detritylation / 3.1: Ring cleavage;
DOI:10.1016/S0960-894X(00)00473-X

Reference yield:

: 36116-18-4
cyclopropyl 4-hydroxyphenyl ketone

: 184027-48-3
4-Hydroxy-1-(4-(3-(1H-imidazol-4-yl)propyloxy)phenyl)butanone ethylene acetal

Guidance literature:: Multi-step reaction with 3 steps

1: Ph₃P; DEAD / tetrahydrofuran

2: aq. HCl / tetrahydrofuran / Heating

3: p-TsOH / Heating

With hydrogenchloride; toluene-4-sulfonic acid; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 1: Mitsunobu reaction / 2: detritylation / 3: Ring cleavage;
DOI:10.1016/S0960-894X(00)00473-X

Reference yield:

: 772-31-6
cyclopropyl(4-fluorophenyl)methanone

: 184027-48-3
4-Hydroxy-1-(4-(3-(1H-imidazol-4-yl)propyloxy)phenyl)butanone ethylene acetal

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / toluene

1.2: toluene / Heating

2.1: aq. HCl / tetrahydrofuran / Heating

3.1: p-TsOH / Heating

With hydrogenchloride; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; toluene; 1.1: Metallation / 1.2: Etherification / 2.1: detritylation / 3.1: Ring cleavage;
DOI:10.1016/S0960-894X(00)00473-X