C₃₉H₄₅NO₅Si

Base Information

• Chemical Name: C₃₉H₄₅NO₅Si
• CAS No.: 1374647-12-7
• Molecular Formula: C₃₉H₄₅NO₅Si
• Molecular Weight: 635.875
• Mol file: 1374647-12-7.mol

Synonyms:

Chemical Property of C₃₉H₄₅NO₅Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₉H₄₅NO₅Si

There total 4 articles about C₃₉H₄₅NO₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-carboxybenzophenone (611-95-0) → C39H45NO5Si (1374647-12-7)

Guidance literature:

Multi-step reaction with 3 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

2: water; lithium hydroxide / 1,2-dimethoxyethane

3: 1H-imidazole / N,N-dimethyl-formamide

With 1H-imidazole; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In 1,2-dimethoxyethane; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2012.02.027

Reference yield:

C19H21NO2 (777016-09-8) → C39H45NO5Si (1374647-12-7)

Guidance literature:

Multi-step reaction with 3 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

2: water; lithium hydroxide / 1,2-dimethoxyethane

3: 1H-imidazole / N,N-dimethyl-formamide

With 1H-imidazole; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In 1,2-dimethoxyethane; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2012.02.027

Reference yield:

C33H29NO4 (1374647-11-6) → C39H45NO5Si (1374647-12-7)

Guidance literature:

Multi-step reaction with 2 steps

1: water; lithium hydroxide / 1,2-dimethoxyethane

2: 1H-imidazole / N,N-dimethyl-formamide

With 1H-imidazole; water; lithium hydroxide; In 1,2-dimethoxyethane; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2012.02.027

upstream raw materials:

C₁₉H₂₁NO₂

tert-butyldimethylsilyl chloride

C₃₃H₂₉NO₄

4-carboxybenzophenone

Downstream raw materials:

C₅₄H₆₀N₄O₆

C₆₀H₇₄N₄O₆Si