BrH*C₂₈H₂₅NO₂

Base Information

Chemical Name:BrH*C₂₈H₂₅NO₂
CAS No.:1005456-20-1
Molecular Formula:BrH*C₂₈H₂₅NO₂
Molecular Weight:488.424
Hs Code.:

BrH*C<sub>28</sub>H<sub>25</sub>NO<sub>2</sub>

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Chemical Property of BrH*C₂₈H₂₅NO₂

Chemical Property:

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Technology Process of BrH*C₂₈H₂₅NO₂

There total 10 articles about BrH*C₂₈H₂₅NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₀H₂₉NO₂

: 1005456-20-1
BrH*C₂₈H₂₅NO₂

Guidance literature:: With boron tribromide; In dichloromethane; at -70 - 20 ℃;

Reference yield:

: 37859-24-8
2-(4-bromophenyl)acetyl chloride

: 1005456-20-1
BrH*C₂₈H₂₅NO₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium hydroxide / dichloromethane; water / 20 °C

2.1: trichlorophosphate / acetonitrile / 5 h / Heating / reflux

2.2: 20 °C

3.1: sodium hydroxide / dichloromethane; water / 20 °C

4.1: hydrogenchloride / methanol; diethyl ether

5.1: dmap; triethylamine / DMF (N,N-dimethyl-formamide); dichloromethane / 0 - 20 °C

6.1: Resolution of racemate

7.1: hydrogen bromide / acetic acid / 20 °C

8.1: sodium carbonate; triphenylphosphine / palladium diacetate / isopropyl alcohol / Heating / reflux

9.1: boron tribromide / dichloromethane / -70 - 20 °C

With hydrogenchloride; dmap; sodium hydroxide; sodium carbonate; hydrogen bromide; boron tribromide; triethylamine; triphenylphosphine; trichlorophosphate; palladium diacetate; In methanol; DMF (N,N-dimethyl-formamide); diethyl ether; dichloromethane; water; acetic acid; isopropyl alcohol; acetonitrile;

Reference yield:

: 1005456-39-2
C₂₉H₃₈BrNO₄

: 1005456-20-1
BrH*C₂₈H₂₅NO₂

Guidance literature:: Multi-step reaction with 4 steps

1: Resolution of racemate

2: hydrogen bromide / acetic acid / 20 °C

3: sodium carbonate; triphenylphosphine / palladium diacetate / isopropyl alcohol / Heating / reflux

4: boron tribromide / dichloromethane / -70 - 20 °C

With sodium carbonate; hydrogen bromide; boron tribromide; triphenylphosphine; palladium diacetate; In dichloromethane; acetic acid; isopropyl alcohol;