Technology Process of 3,5-Dibenzyloxy-1-hydroxy-2,4-bis(3,3-dimethylallyl)acridone
There total 7 articles about 3,5-Dibenzyloxy-1-hydroxy-2,4-bis(3,3-dimethylallyl)acridone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 900 mg / methanol; diethyl ether / 12 h / 0 °C
2: 10 mg / conc. H2SO4 / 12 h
3: 4 g / NaHCO3, NaI / acetone / 18 h / Heating
4: 200 mg / BF3 etherate / dioxane / 2 h
5: 50 mg / NaI, K2CO3 / acetone / 6 h / Heating
With
sulfuric acid; boron trifluoride diethyl etherate; sodium hydrogencarbonate; potassium carbonate; sodium iodide;
In
1,4-dioxane; methanol; diethyl ether; acetone;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 200 mg / BF3 etherate / dioxane / 2 h
2: 50 mg / NaI, K2CO3 / acetone / 6 h / Heating
With
boron trifluoride diethyl etherate; potassium carbonate; sodium iodide;
In
1,4-dioxane; acetone;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 4 g / NaHCO3, NaI / acetone / 18 h / Heating
2: 200 mg / BF3 etherate / dioxane / 2 h
3: 50 mg / NaI, K2CO3 / acetone / 6 h / Heating
With
boron trifluoride diethyl etherate; sodium hydrogencarbonate; potassium carbonate; sodium iodide;
In
1,4-dioxane; acetone;