(5-[4-(3,4-dicyanophenoxy)phenyl]-10,15,20-triphenylporphyrinato)cobalt(II)

Base Information

Chemical Name:(5-[4-(3,4-dicyanophenoxy)phenyl]-10,15,20-triphenylporphyrinato)cobalt(II)
CAS No.:851165-72-5
Molecular Formula:C₅₂H₃₀CoN₆O
Molecular Weight:813.843
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (5-[4-(3,4-dicyanophenoxy)phenyl]-10,15,20-triphenylporphyrinato)cobalt(II)

Chemical Property:

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Technology Process of (5-[4-(3,4-dicyanophenoxy)phenyl]-10,15,20-triphenylporphyrinato)cobalt(II)

There total 1 articles about (5-[4-(3,4-dicyanophenoxy)phenyl]-10,15,20-triphenylporphyrinato)cobalt(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.5%

: 5-[4-(3,4-dicyanophenoxy)phenyl]-10,15,20-triphenylporphyrin

: 6147-53-1
cobalt(II) diacetate tetrahydrate

: 851165-72-5
(5-[4-(3,4-dicyanophenoxy)phenyl]-10,15,20-triphenylporphyrinato)cobalt(II)

Guidance literature:: In N,N-dimethyl-formamide; byproducts: acetic acid; (N2); heating a mixt. of ligand and cobalt salt in DMF to 70°C for 2 h with stirring, cooling to room temp.; addn. to CH2Cl2, washing with water, column chromy. (silica gel, CH2Cl2), evapn., recrystn. (CH2Cl2/methanol);
DOI:10.1039/b418611g

Reference yield:

: 851165-72-5
(5-[4-(3,4-dicyanophenoxy)phenyl]-10,15,20-triphenylporphyrinato)cobalt(II)

: 7664-41-7
ammonia

: Co(C₅H₂N)4(C₆H₅)3C₆H₄OC₆H₃CNHNHCNH

Guidance literature:: With sodium methylate; In methanol; bubbling NH3 through a suspn. of cobalt complex with sodium methoxide inmethanol for 1 h, refluxing for 6 h with bubbling NH3; evapn.;
DOI:10.1039/b418611g