C₁₈H₃₁N₃O₂

Base Information

Chemical Name:C₁₈H₃₁N₃O₂
CAS No.:1380601-41-1
Molecular Formula:C₁₈H₃₁N₃O₂
Molecular Weight:321.463
Hs Code.:

C<sub>18</sub>H<sub>31</sub>N<sub>3</sub>O<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₃₁N₃O₂

Chemical Property:

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Technology Process of C₁₈H₃₁N₃O₂

There total 1 articles about C₁₈H₃₁N₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 446-35-5
2,4-Difluoronitrobenzene

: 1380601-41-1
C₁₈H₃₁N₃O₂

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / water / 4 h / 50 °C / Cooling with ice

2: potassium carbonate / N,N-dimethyl acetamide / 18 h / Reflux

With potassium carbonate; triethylamine; In N,N-dimethyl acetamide; water;
DOI:10.1080/00397911.2011.564342

Reference yield:

: 1380601-41-1
C₁₈H₃₁N₃O₂

: 1380601-42-2
2-isobutylamino-4-(di-(n-butyl)amino)aniline

Guidance literature:: With 5%-palladium/activated carbon; hydrogen; acetic acid; In ethanol; for 5h; under 2585.81 Torr;
DOI:10.1080/00397911.2011.564342

Reference yield:

: 1380601-41-1
C₁₈H₃₁N₃O₂

: (E)-2-(3-cyano-4-(2-(6-(di-(n-butyl)amino)-1-iso-butyl-1H-benzimidazole-2-yl))vinyl)-5,5-dimethylfuran-2(5H)-ylidene malononitrile

Guidance literature:: Multi-step reaction with 4 steps

1.1: 5%-palladium/activated carbon; hydrogen; acetic acid / ethanol / 5 h / 2585.81 Torr

2.1: toluene-4-sulfonic acid / N,N-dimethyl acetamide / 1 h / 80 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.67 h / -20 °C / Inert atmosphere; Cooling with acetone-dry ice

3.2: 2.67 h / 20 °C / Cooling with acetone-dry ice; Inert atmosphere

4.1: piperdinium acetate / ethanol / 0.5 h / Reflux

With n-butyllithium; 5%-palladium/activated carbon; hydrogen; piperdinium acetate; toluene-4-sulfonic acid; acetic acid; In tetrahydrofuran; ethanol; hexane; N,N-dimethyl acetamide;
DOI:10.1080/00397911.2011.564342