Technology Process of (+)-dichloro-1,1'-(2,3-O-isopropylidene-2,3-dihydroxybutane-1,4-dioxy)-3,3',4,4'-tetramethyl-5,5'-diphenyl-2,2'-biphosphole platinum(II)
There total 1 articles about (+)-dichloro-1,1'-(2,3-O-isopropylidene-2,3-dihydroxybutane-1,4-dioxy)-3,3',4,4'-tetramethyl-5,5'-diphenyl-2,2'-biphosphole platinum(II) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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In
dichloromethane;
(Ar), diphosphinite in CH2Cl2 treated with 1 equiv. of Pt complex, stirred at room temp. for 3 h; filtered, concd.(vac.), dissolved (CH2Cl2), pptd.(large excess of pentane), filtered, dried (vac.);
DOI:10.1016/j.ica.2007.09.043