C₄₅H₅₅ClN₂O₁₂

Base Information

• Chemical Name: C₄₅H₅₅ClN₂O₁₂
• CAS No.: 1408300-69-5
• Molecular Formula: C₄₅H₅₅ClN₂O₁₂
• Molecular Weight: 851.391
• Mol file: 1408300-69-5.mol

Synonyms:

Chemical Property of C₄₅H₅₅ClN₂O₁₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₄₅H₅₅ClN₂O₁₂

There total 2 articles about C₄₅H₅₅ClN₂O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C45H53ClN2O12 → C45H55ClN2O12 (1408300-69-5)

Guidance literature:

With sodium cyanoborohydride; In ethanol; dichloromethane; at 20 ℃; for 0.0166667h;

DOI:10.1039/c2ob26317c

Reference yield:

rifampicin (13292-46-1) → C45H55ClN2O12 (1408300-69-5)

Guidance literature:

Multi-step reaction with 3 steps

1: hydrogenchloride / water; diethyl ether / 96 h / 20 °C

2: hydrogenchloride / dichloromethane; ethanol / 0.5 h / 45 °C

3: sodium cyanoborohydride / dichloromethane; ethanol / 0.02 h / 20 °C

With hydrogenchloride; sodium cyanoborohydride; In diethyl ether; ethanol; dichloromethane; water;

DOI:10.1039/c2ob26317c

upstream raw materials:

rifampicin

Refernces