C₂₂H₂₀F₉N₇

Base Information

Chemical Name:C₂₂H₂₀F₉N₇
CAS No.:867012-72-4
Molecular Formula:C₂₂H₂₀F₉N₇
Molecular Weight:553.433
Hs Code.:

C<sub>22</sub>H<sub>20</sub>F<sub>9</sub>N<sub>7</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₀F₉N₇

Chemical Property:

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Technology Process of C₂₂H₂₀F₉N₇

There total 10 articles about C₂₂H₂₀F₉N₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₅H₂₀F₃N₃O₂

: 867012-72-4
C₂₂H₂₀F₉N₇

Guidance literature:: Multi-step reaction with 6 steps

1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C

2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

3: sodium azide; triethylamine / toluene / 110 °C

4: potassium carbonate / acetonitrile

5: Chiralpak AD / Resolution of racemate

6: sulfuric acid; trifluoroacetic acid / 0 - 20 °C

With sodium azide; sulfuric acid; sodium tris(acetoxy)borohydride; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; 1,2-dichloro-ethane; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.075

Reference yield:

: 867011-80-1
(2R,4S)-isopropyl 4-((3,5-bis(trifluoromethyl)benzyl)(2-methyl-2H-tetrazol-5-yl)amino)-2-ethyl-6-(trifluoromethyl)-3,4-dihydro-1,5-naphthyridine-1(2H)-carboxylate.

: 867012-72-4
C₂₂H₂₀F₉N₇

Guidance literature:: With sulfuric acid; trifluoroacetic acid; at 0 - 20 ℃;
DOI:10.1016/j.bmcl.2012.03.075

Reference yield:

: C₁₃H₁₆F₃N₃O

: 867012-72-4
C₂₂H₂₀F₉N₇

Guidance literature:: Multi-step reaction with 8 steps

1: pyridine / 0 - 20 °C

2: hydrogenchloride / water / 80 °C

3: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C

4: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

5: sodium azide; triethylamine / toluene / 110 °C

6: potassium carbonate / acetonitrile

7: Chiralpak AD / Resolution of racemate

8: sulfuric acid; trifluoroacetic acid / 0 - 20 °C

With pyridine; hydrogenchloride; sodium azide; sulfuric acid; sodium tris(acetoxy)borohydride; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; water; 1,2-dichloro-ethane; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.075