RuCl(η3-allyl)(CO)(1,1'-bis(diphenylphosphino)ferrocene)

Base Information

Chemical Name:RuCl(η3-allyl)(CO)(1,1'-bis(diphenylphosphino)ferrocene)
CAS No.:640721-13-7
Molecular Formula:C₃₈H₃₃ClFeOP₂Ru
Molecular Weight:759.997
Hs Code.:

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Chemical Property of RuCl(η3-allyl)(CO)(1,1'-bis(diphenylphosphino)ferrocene)

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Technology Process of RuCl(η3-allyl)(CO)(1,1'-bis(diphenylphosphino)ferrocene)

There total 1 articles about RuCl(η3-allyl)(CO)(1,1'-bis(diphenylphosphino)ferrocene) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 12150-46-8
1,1'-bis-(diphenylphosphino)ferrocene

: 114925-37-0
(η3-C3H5)Ru(CO)3Cl

: 640721-13-7
RuCl(η3-allyl)(CO)(1,1'-bis(diphenylphosphino)ferrocene)

Guidance literature:: In toluene; N2; adding 1 equiv. of diphosphine to toluene soln. of Ru complex at room temp., refluxing for 3 h; evapn. to dryness, dissolving the residue in CH2Cl2, chromy. (neutral Al2O3, methanol), solvent removal; elem. anal.;
DOI:10.1021/om030530e

Reference yield: 88.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 640721-13-7
RuCl(η3-allyl)(CO)(1,1'-bis(diphenylphosphino)ferrocene)

: [RuCl(μ-Cl)(CO)(1,1'-bis(diphenylphosphino)ferrocene)]2

Guidance literature:: In diethyl ether; dichloromethane; N2; adding 1.5 equiv. of HCl in diethyl ether (1.0 M) to dichloromethanesoln. of Ru complex, stirring at room temp. for 30 min; evapn. to dryness, washing the solid with diethyl ether, vac. drying; elem. anal.;
DOI:10.1021/om030530e