Technology Process of C34H48N4O12S
There total 8 articles about C34H48N4O12S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: water / 100 °C
2: isopropyl alcohol / water / 65 °C
3: Alkaline conditions
4: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / dichloromethane; water
5: sodium methylate; methanol
6: pyridine
7: pyridine; sulfur trioxide pyridine complex / 45 °C
With
pyridine; methanol; water; sodium methylate; tetra(n-butyl)ammonium hydrogensulfate; sulfur trioxide pyridine complex; isopropyl alcohol; sodium hydroxide;
In
dichloromethane; water;
2: |Michael Addition;
DOI:10.1021/ac5004135
- Guidance literature:
-
Multi-step reaction with 7 steps
1: sodium hydrogencarbonate / dichloromethane; water
2: isopropyl alcohol / water / 65 °C
3: Alkaline conditions
4: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / dichloromethane; water
5: sodium methylate; methanol
6: pyridine
7: pyridine; sulfur trioxide pyridine complex / 45 °C
With
pyridine; methanol; sodium methylate; tetra(n-butyl)ammonium hydrogensulfate; sulfur trioxide pyridine complex; sodium hydrogencarbonate; isopropyl alcohol; sodium hydroxide;
In
dichloromethane; water;
2: |Michael Addition;
DOI:10.1021/ac5004135
- Guidance literature:
-
Multi-step reaction with 5 steps
1: Alkaline conditions
2: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / dichloromethane; water
3: sodium methylate; methanol
4: pyridine
5: pyridine; sulfur trioxide pyridine complex / 45 °C
With
pyridine; methanol; sodium methylate; tetra(n-butyl)ammonium hydrogensulfate; sulfur trioxide pyridine complex; sodium hydroxide;
In
dichloromethane; water;
DOI:10.1021/ac5004135