2-ethyl 5-(5,5-dimethyl-2-oxo-1,3,2-dioxaphosphorinan-2-yl)-1,4-dihydro-2,6-dimethyl-4-(2-trifluoromethylphenyl)-3-pyridinecarboxylate

Base Information

Chemical Name:2-ethyl 5-(5,5-dimethyl-2-oxo-1,3,2-dioxaphosphorinan-2-yl)-1,4-dihydro-2,6-dimethyl-4-(2-trifluoromethylphenyl)-3-pyridinecarboxylate
CAS No.:98908-21-5
Molecular Formula:C₃₀H₃₆F₃N₂O₅P
Molecular Weight:592.595
Hs Code.:

2-<benzyl(methyl)amino>ethyl 5-(5,5-dimethyl-2-oxo-1,3,2-dioxaphosphorinan-2-yl)-1,4-dihydro-2,6-dimethyl-4-(2-trifluoromethylphenyl)-3-pyridinecarboxylate

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Chemical Property of 2-ethyl 5-(5,5-dimethyl-2-oxo-1,3,2-dioxaphosphorinan-2-yl)-1,4-dihydro-2,6-dimethyl-4-(2-trifluoromethylphenyl)-3-pyridinecarboxylate

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Technology Process of 2-ethyl 5-(5,5-dimethyl-2-oxo-1,3,2-dioxaphosphorinan-2-yl)-1,4-dihydro-2,6-dimethyl-4-(2-trifluoromethylphenyl)-3-pyridinecarboxylate

There total 5 articles about 2-ethyl 5-(5,5-dimethyl-2-oxo-1,3,2-dioxaphosphorinan-2-yl)-1,4-dihydro-2,6-dimethyl-4-(2-trifluoromethylphenyl)-3-pyridinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 54527-73-0
2-ethyl 3-aminocrotonate

: 124727-71-5
2-<1-acetyl-2-(2-trifluoromethylphenyl)ethenyl>-5,5-dimethyl-2-oxo-1,3,2-dioxaphosphorinane

: 98908-21-5
2-ethyl 5-(5,5-dimethyl-2-oxo-1,3,2-dioxaphosphorinan-2-yl)-1,4-dihydro-2,6-dimethyl-4-(2-trifluoromethylphenyl)-3-pyridinecarboxylate

Guidance literature:: In toluene; for 9h; Heating;
DOI:10.1248/cpb.40.2362

Reference yield:

: 115578-88-6
(E)-2,2-dimethyl-1,3-propanediyl α-acetyl-2-(trifluoromethyl)styrylphosphonate

: 98908-21-5
2-ethyl 5-(5,5-dimethyl-2-oxo-1,3,2-dioxaphosphorinan-2-yl)-1,4-dihydro-2,6-dimethyl-4-(2-trifluoromethylphenyl)-3-pyridinecarboxylate

Guidance literature:

Reference yield:

: 1005-69-2
2-methoxy-5,5-dimethyl-1,3,2-dioxaphosphorinane

: 98908-21-5
2-ethyl 5-(5,5-dimethyl-2-oxo-1,3,2-dioxaphosphorinan-2-yl)-1,4-dihydro-2,6-dimethyl-4-(2-trifluoromethylphenyl)-3-pyridinecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 65.8 percent / diethyl ether / 7 h / Heating

2: 42 percent / piperidine, trifluoroacetic acid / toluene / 8 h / Heating

3: 59 percent / toluene / 9 h / Heating

With piperidine; trifluoroacetic acid; In diethyl ether; toluene;
DOI:10.1248/cpb.40.2362