cis-1,4-Dihydro-3,5-dimethyl-1,4-diphenyl-1,4-phospharsinin

Base Information

Chemical Name:cis-1,4-Dihydro-3,5-dimethyl-1,4-diphenyl-1,4-phospharsinin
CAS No.:97972-25-3
Molecular Formula:C₁₈H₁₈AsP
Molecular Weight:340.236
Hs Code.:

Synonyms:

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Chemical Property of cis-1,4-Dihydro-3,5-dimethyl-1,4-diphenyl-1,4-phospharsinin

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Technology Process of cis-1,4-Dihydro-3,5-dimethyl-1,4-diphenyl-1,4-phospharsinin

There total 4 articles about cis-1,4-Dihydro-3,5-dimethyl-1,4-diphenyl-1,4-phospharsinin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 644-97-3
Dichlorophenylphosphine

: 97972-25-3,97972-26-4
trans-1,4-Dihydro-3,5-dimethyl-1,4-diphenyl-1,4-phospharsinin

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / EtMgBr / tetrahydrofuran; diethyl ether / 1.) 2 h, 25 deg C, 2.) 30 min., reflux

2: Li, liq. NH₃, Fe(NO₃)3 / tetrahydrofuran / 1 h

With ethylmagnesium bromide; ammonia; lithium; ferric nitrate; In tetrahydrofuran; diethyl ether;

Reference yield:

: 644-97-3
Dichlorophenylphosphine

: 97972-25-3,97972-26-4
cis-1,4-Dihydro-3,5-dimethyl-1,4-diphenyl-1,4-phospharsinin

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / EtMgBr / tetrahydrofuran; diethyl ether / 1.) 2 h, 25 deg C, 2.) 30 min., reflux

2: Li, liq. NH₃, Fe(NO₃)3 / tetrahydrofuran / 1 h

With ethylmagnesium bromide; ammonia; lithium; ferric nitrate; In tetrahydrofuran; diethyl ether;

Reference yield:

: 39997-80-3
phenylbis(1-propynyl)phosphane

: 822-65-1
phenylarsane

: 97972-25-3,97972-26-4
trans-1,4-Dihydro-3,5-dimethyl-1,4-diphenyl-1,4-phospharsinin

: 97972-25-3,97972-26-4
cis-1,4-Dihydro-3,5-dimethyl-1,4-diphenyl-1,4-phospharsinin

Guidance literature:: With ammonia; lithium; ferric nitrate; In tetrahydrofuran; for 1h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;