phenylbis(1-propynyl)phosphane

Base Information

Chemical Name:phenylbis(1-propynyl)phosphane
CAS No.:39997-80-3
Molecular Formula:C₁₂H₁₁P
Molecular Weight:186.193
Hs Code.:

Synonyms:phenylbis(1-propynyl)phosphane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenylbis(1-propynyl)phosphane

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Technology Process of phenylbis(1-propynyl)phosphane

There total 2 articles about phenylbis(1-propynyl)phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 644-97-3
Dichlorophenylphosphine

: 74-99-7
prop-1-yne

: 39997-80-3
phenylbis(1-propynyl)phosphane

Guidance literature:: With ethylmagnesium bromide; In tetrahydrofuran; diethyl ether; 1.) 2 h, 25 deg C, 2.) 30 min., reflux;

Reference yield: 66.0%

: 4529-04-8
1-propynyl lithium

: 644-97-3
Dichlorophenylphosphine

: 39997-80-3
phenylbis(1-propynyl)phosphane

Guidance literature:: With phosphorus trichloride; In tetrahydrofuran; for 1h;
DOI:10.1002/chem.200700649

Reference yield: 97.0%

: 37366-09-9
dichloro(benzene)ruthenium(II) dimer

: 39997-80-3
phenylbis(1-propynyl)phosphane

: 1194043-55-4
[Ru(η6-C6H6)(PPh(CCCH3)2)Cl2]

Guidance literature:: In acetone; (Ar); std. Schlenk technique; Ru complex was added to soln. of P ligand in acetone; stirred for 1 d; evapd.; washed (hexane); dried (vac.);
DOI:10.1021/om900502a