(CH₃OC₆H₄NCHC₄H₃N)2TiCl₂

Base Information

Chemical Name:(CH₃OC₆H₄NCHC₄H₃N)2TiCl₂
CAS No.:274687-49-9
Molecular Formula:C₂₄H₂₂Cl₂N₄O₂Ti
Molecular Weight:517.25
Hs Code.:

(CH<sub>3</sub>OC<sub>6</sub>H<sub>4</sub>NCHC<sub>4</sub>H<sub>3</sub>N)2TiCl<sub>2</sub>

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Chemical Property of (CH₃OC₆H₄NCHC₄H₃N)2TiCl₂

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Technology Process of (CH₃OC₆H₄NCHC₄H₃N)2TiCl₂

There total 1 articles about (CH₃OC₆H₄NCHC₄H₃N)2TiCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 80525-78-6
N-((1H-pyrrol-2-yl)-methylene)-4-methoxyaniline

: 7550-45-0
titanium tetrachloride

: 274687-49-9
(CH₃OC₆H₄NCHC₄H₃N)2TiCl₂

Guidance literature:: With n-butyl lithium; In diethyl ether; hexane; n-heptane; under N2, standard Schlenk techniques; hexane soln. of n-BuLi added (5 min) to stirred soln. of ligand (2 equiv.) in Et2O at -78°C; stirred (room temp., 4 h); added (30 min) to n-heptane soln. of TiCl4 at -78°C; stirred (room temp., 12 h); filtered through glass filter; filtrate concd. in vac.; Et2O added to solid; stirred for 10 min; filtered; filtrate concd. in vac.; CH2Cl2 and n-hexane added to solid; stirred for 1 h; filtered; solvent evapd.; elem.anal.;
DOI:10.1021/om010468q