2-(diphenylhydroxymethyl)-1,1'-N,N,N',N'-tetraisopropylferrocenedicarboxamide

Base Information

Chemical Name:2-(diphenylhydroxymethyl)-1,1'-N,N,N',N'-tetraisopropylferrocenedicarboxamide
CAS No.:896445-28-6
Molecular Formula:C₃₇H₄₆FeN₂O₃
Molecular Weight:622.631
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(diphenylhydroxymethyl)-1,1'-N,N,N',N'-tetraisopropylferrocenedicarboxamide

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Technology Process of 2-(diphenylhydroxymethyl)-1,1'-N,N,N',N'-tetraisopropylferrocenedicarboxamide

There total 1 articles about 2-(diphenylhydroxymethyl)-1,1'-N,N,N',N'-tetraisopropylferrocenedicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 119-61-9
benzophenone

: 261618-64-8
2-(tributylstannyl)-1,1'-N,N,N',N'-tetraisopropylferrocenedicarboxamide

: 896445-28-6,261618-62-6
2-(diphenylhydroxymethyl)-1,1'-N,N,N',N'-tetraisopropylferrocenedicarboxamide

Guidance literature:: With n-butyllithium; In hexane; toluene; addn. of soln. of BuLi in hexane to a stirred soln. of ferrocene derivative in toluene at -78 °C under Ar, stirring for 15 min at -78 °C, addn. of Ph2CO in toluene, stirring for 40 min at -78 °C,; addn. of water or aq. NH4Cl, extracton with ether, drying over MgSO4, filtration, concn. under reduced pressure, chromatography on silica gel (EtOAc-hexane 8:1);
DOI:10.1139/V06-008