Technology Process of C31H34O6
There total 13 articles about C31H34O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C31H32O5;
With
boron trifluoride-tetrahydrofuran complex;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 1h;
With
dihydrogen peroxide; sodium hydroxide;
In
tetrahydrofuran; water;
at 20 ℃;
for 3h;
regioselective reaction;
DOI:10.1021/jo2019762
- Guidance literature:
-
With
diisobutylaluminium hydride;
In
dichloromethane; toluene;
at -78 ℃;
for 0.5h;
regioselective reaction;
DOI:10.1021/jo2019762
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: ozone / dichloromethane / -78 °C
1.2: 20 °C
2.1: chromium dichloride / tetrahydrofuran / 0 °C
3.1: chromium dichloride; nickel dichloride / dimethyl sulfoxide
4.1: acetic acid / water / 60 °C
5.1: dichloro bis(acetonitrile) palladium(II) / tetrahydrofuran / 6 h / 20 °C
6.1: lithium hydroxide / 1,4-dioxane; water / 80 °C
7.1: dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine / tetrahydrofuran; toluene
8.1: boron trifluoride-tetrahydrofuran complex / tetrahydrofuran / 1 h / 0 - 20 °C
8.2: 3 h / 20 °C
With
chromium dichloride; dmap; dichloro bis(acetonitrile) palladium(II); boron trifluoride-tetrahydrofuran complex; 2,4,6-trichlorobenzoyl chloride; ozone; acetic acid; triethylamine; nickel dichloride; lithium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water; dimethyl sulfoxide; toluene;
2.1: Takai iodoalkenylation / 3.1: Nozaki-Hiyama-Kishi coupling / 7.1: Yamaguchi macrolactonization;
DOI:10.1021/jo2019762
