(E)-2-triphenylstannyl-2-tridecene

Base Information

Chemical Name:(E)-2-triphenylstannyl-2-tridecene
CAS No.:120978-46-3
Molecular Formula:C₃₁H₄₀Sn
Molecular Weight:531.369
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-2-triphenylstannyl-2-tridecene

Chemical Property:

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Technology Process of (E)-2-triphenylstannyl-2-tridecene

There total 2 articles about (E)-2-triphenylstannyl-2-tridecene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 52629-63-7
trideca-1,2-diene

: 892-20-6
triphenylstannane

: 120978-49-6
(E)-1-triphenylstannyl-2-tridecene

: 120978-48-5
2-triphenylstannyl-1-tridecene

: 120978-46-3,120978-47-4
(Z)-2-triphenylstannyl-2-tridecene

: 120978-46-3,120978-47-4
(E)-2-triphenylstannyl-2-tridecene

Guidance literature:: triethyl borane; In hexane; benzene; Ar atmosphere, addn. of catalyst BEt3 in hexane to soln. of allene and HSnPh3 in benzene, stirring (25°C, 2 h); pouring of reaction mixt. into water, extraction (ethyl acetate), chromy. (preperative TLC); mixt. of (Z)-/(E)-2-SnPh3-2-tridecene (total yield 51%) and 2-SnPh3-1-tridecene not separated; (E)-1-SnPh3-2-tridecene isolated in pure form; elem. anal.;
DOI:10.1246/bcsj.61.2693

Reference yield: 10.0%

: 52629-63-7
trideca-1,2-diene

: 892-20-6
triphenylstannane

: 120978-49-6
(E)-1-triphenylstannyl-2-tridecene

: 120978-48-5
2-triphenylstannyl-1-tridecene

: 120978-46-3,120978-47-4
(Z)-2-triphenylstannyl-2-tridecene

: 120978-46-3,120978-47-4
(E)-2-triphenylstannyl-2-tridecene

Guidance literature:: triethyl borane; In hexane; benzene; Ar atmosphere, addn. of catalyst BEt3 in hexane to soln. of allene and HSnPh3 in benzene, stirring (25°C, 2 h); pouring of reaction mixt. into water, extraction (ethyl acetate), chromy. (preperative TLC); mixt. of (Z)-/(E)-2-SnPh3-2-tridecene (total yield 51%) and 2-SnPh3-1-tridecene not separated; (E)-1-SnPh3-2-tridecene isolated in pure form; elem. anal.;
DOI:10.1246/bcsj.61.2693