1-(diphenylphosphino)-1'-(N-[(2-pyridyl)methyl]carbamoyl)ferrocene

Base Information

Chemical Name:1-(diphenylphosphino)-1'-(N-[(2-pyridyl)methyl]carbamoyl)ferrocene
CAS No.:946507-58-0
Molecular Formula:C₂₉H₂₅FeN₂OP
Molecular Weight:504.351
Hs Code.:

Synonyms:

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Chemical Property of 1-(diphenylphosphino)-1'-(N-[(2-pyridyl)methyl]carbamoyl)ferrocene

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Technology Process of 1-(diphenylphosphino)-1'-(N-[(2-pyridyl)methyl]carbamoyl)ferrocene

There total 1 articles about 1-(diphenylphosphino)-1'-(N-[(2-pyridyl)methyl]carbamoyl)ferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 3731-51-9
2-(Aminomethyl)pyridine

: 173346-69-5
1′-(diphenylphosphino)ferrocene-1-carboxylic acid

: 946507-58-0
1-(diphenylphosphino)-1'-(N-[(2-pyridyl)methyl]carbamoyl)ferrocene

Guidance literature:: With 1-hydroxybenzotriazole; N-(3-Dimethylaminopropyl)-N'ethylcarbodiimide; In dichloromethane; addn. of carbodiimide derivative to a stirred soln. of ferrocene derivative and 1-hydroxybenzatriazole under Ar, excluding direct daylight, stirring for 30 min at 0 °C, addn. of C5H4NCH2NH2, stirring at room temp. overnight; washing with aq. citric acid, satd. aq. NaHCO3, brine, drying over MgSO4, rvapn. under vac., chromy on silica gel with CH2Cl2-methanol (1:1), removal of solvent, recrystn. by layering of hot EtOAc soln. with hexane, elem. anal.;
DOI:10.1039/b701012e

Reference yield: 74.0%

: 946507-58-0
1-(diphenylphosphino)-1'-(N-[(2-pyridyl)methyl]carbamoyl)ferrocene

: mercury dibromide

: [(Hg(μ-Br)Br(Ph2P(ferrocene-1,1'-diyl)C(O)NHCH2(2-C5H4N)-κP))2]

Guidance literature:: In methanol; chloroform; a soln. of Fe-contg. compd. (0.05 mmol) in chloroform was layered with MeOH and then with a MeOH soln. of Hg-contg. compd. (0.05 mmol); after 2 d, crystals were filtered off, washed with MeOH and Et2O and dried under reduced pressure; elem. anal.;
DOI:10.1039/b719334c

Reference yield: 70.0%

: cadmium(II) bromide hexahydrate

: 67-66-3,8013-54-5
chloroform

: 946507-58-0
1-(diphenylphosphino)-1'-(N-[(2-pyridyl)methyl]carbamoyl)ferrocene

: 4Cd⁽²⁺⁾*8Br^(1-)*4Fe⁽²⁺⁾*4C₅H₄P(C₆H₅)2^(1-)*4C₅H₄CONHCH₂C₅H₄N^(1-)*0.3CHCl₃=C₁₁₆H₁₀₀Cd₄Br₈Fe₄N₈O₄P₄*0.3CHCl₃

Guidance literature:: In methanol; chloroform; a soln. of Fe-contg. compd. (0.05 mmol) in chloroform was layered with MeOH and then with a MeOH soln. of Cd-contg. compd. (0.05 mmol); after several days crystals were filtered off, washed with MeOH and Et2Oand dried under reduced pressure; elem. anal.;
DOI:10.1039/b719334c