(Z)-(2RS,3SR)-methyl 2--2,3-methano-4-(diethylphosphinyl)butanoate

Base Information

Chemical Name:(Z)-(2RS,3SR)-methyl 2--2,3-methano-4-(diethylphosphinyl)butanoate
CAS No.:133753-40-9
Molecular Formula:C₁₈H₂₆NO₇P
Molecular Weight:399.381
Hs Code.:

(Z)-(2RS,3SR)-methyl 2-<N-(benzyloxycarbonyl)amino>-2,3-methano-4-(diethylphosphinyl)butanoate

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Chemical Property of (Z)-(2RS,3SR)-methyl 2--2,3-methano-4-(diethylphosphinyl)butanoate

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Technology Process of (Z)-(2RS,3SR)-methyl 2--2,3-methano-4-(diethylphosphinyl)butanoate

There total 9 articles about (Z)-(2RS,3SR)-methyl 2--2,3-methano-4-(diethylphosphinyl)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.3%

: 133753-38-5,133753-39-6
(Z)-(3RS,4RS)-methyl 3--4-<(diethoxyphosphinyl)methyl>pyrazoline-3-carboxylate

: 133753-40-9,133753-41-0
(Z)-(2RS,3SR)-methyl 2--2,3-methano-4-(diethylphosphinyl)butanoate

Guidance literature:: In chloroform; at 20 ℃; for 96h; Irradiation;
DOI:10.1021/jm00109a023

Reference yield: 54.1%

: 133753-38-5,133753-39-6
(E)-(3RS,4SR)-methyl 3--4-<(diethoxyphosphinyl)methyl>pyrazoline-3-carboxylate

: 133753-40-9,133753-41-0
(E)-(2RS,3RS)-methyl 2--2,3-methano-4-(diethylphosphinyl)butanoate

Guidance literature:: In chloroform; at 20 ℃; for 70h; Irradiation;
DOI:10.1021/jm00109a023

Reference yield:

: 1606-75-3
(2-oxoethyl)phosphonic acid diethyl ester

: 133753-40-9,133753-41-0
(E)-(2RS,3RS)-methyl 2--2,3-methano-4-(diethylphosphinyl)butanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) potassium tert-butoxide / 1.) CH₂Cl₂, -78 deg C, 20 min, 2.) CH₂Cl₂, RT, 2 h

2: 88 percent / diethyl ether / 72 h / Ambient temperature

3: 54.1 percent / CHCl₃ / 70 h / 20 °C / Irradiation

With potassium tert-butylate; In diethyl ether; chloroform;
DOI:10.1021/jm00109a023