C₁₆H₂₀N₂O₅S

Base Information

Chemical Name:C₁₆H₂₀N₂O₅S
CAS No.:1397758-42-7
Molecular Formula:C₁₆H₂₀N₂O₅S
Molecular Weight:352.411
Hs Code.:

C<sub>16</sub>H<sub>20</sub>N<sub>2</sub>O<sub>5</sub>S

Synonyms:

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Chemical Property of C₁₆H₂₀N₂O₅S

Chemical Property:

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Technology Process of C₁₆H₂₀N₂O₅S

There total 7 articles about C₁₆H₂₀N₂O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1383736-53-5
(4R,5R)-methyl 5-methyl-4-(pent-4-en-1-yl)-2-phenyl-4,5-dihydrooxazole-4-carboxylate

: 1397758-42-7
C₁₆H₂₀N₂O₅S

Guidance literature:: Multi-step reaction with 6 steps

1.1: N,O-dimethylhydroxylamine*hydrochloride / tetrahydrofuran / 0.08 h / Inert atmosphere

1.2: -5 - 20 °C / Inert atmosphere

2.1: ozone / ethyl acetate / -78 °C

2.2: 8 h / Inert atmosphere; Reflux

3.1: silica gel; N-ethyl-N,N-diisopropylamine / toluene / 48 h / 75 °C

4.1: sodium tetrahydroborate / methanol

5.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane

6.1: sodium hydride / acetonitrile

With sodium tetrahydroborate; N,O-dimethylhydroxylamine*hydrochloride; silica gel; sodium hydride; sodium hydrogencarbonate; ozone; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; toluene; acetonitrile; 3.1: Aldol condensation;
DOI:10.1021/ol301461e

Reference yield:

: 1383736-52-4
4-((4R,5R)-4-acetyl-5-methyl-2-phenyl-4,5-dihydrooxazol-4-yl)butanal

: 1397758-42-7
C₁₆H₂₀N₂O₅S

Guidance literature:: Multi-step reaction with 4 steps

1: silica gel; N-ethyl-N,N-diisopropylamine / toluene / 48 h / 75 °C

2: sodium tetrahydroborate / methanol

3: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane

4: sodium hydride / acetonitrile

With sodium tetrahydroborate; silica gel; sodium hydride; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane; toluene; acetonitrile; 1: Aldol condensation;
DOI:10.1021/ol301461e

Reference yield:

: 1383736-54-6
1-((4R,5R)-5-methyl-4-(pent-4-en-1-yl)-2-phenyl-4,5-dihydrooxazol-4-yl)ethanone

: 1397758-42-7
C₁₆H₂₀N₂O₅S

Guidance literature:: Multi-step reaction with 5 steps

1.1: ozone / ethyl acetate / -78 °C

1.2: 8 h / Inert atmosphere; Reflux

2.1: silica gel; N-ethyl-N,N-diisopropylamine / toluene / 48 h / 75 °C

3.1: sodium tetrahydroborate / methanol

4.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane

5.1: sodium hydride / acetonitrile

With sodium tetrahydroborate; silica gel; sodium hydride; sodium hydrogencarbonate; ozone; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane; ethyl acetate; toluene; acetonitrile; 2.1: Aldol condensation;
DOI:10.1021/ol301461e