phenyl-N-biphenyl-2-ylbenzimidoselenoate

Base Information

Chemical Name:phenyl-N-biphenyl-2-ylbenzimidoselenoate
CAS No.:1083169-35-0
Molecular Formula:C₂₅H₁₉NSe
Molecular Weight:412.393
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl-N-biphenyl-2-ylbenzimidoselenoate

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Technology Process of phenyl-N-biphenyl-2-ylbenzimidoselenoate

There total 2 articles about phenyl-N-biphenyl-2-ylbenzimidoselenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1666-13-3
diphenyl diselenide

: 791811-41-1
N-biphenyl-2-yl-benzimidoyl chloride

: 1083169-35-0
phenyl-N-biphenyl-2-ylbenzimidoselenoate

Guidance literature:: With potassium tri-sec-butyl-borohydride; In tetrahydrofuran; at 20 ℃;
DOI:10.1055/s-2008-1078246

Reference yield:

: 98-88-4
benzoyl chloride

: 1083169-35-0
phenyl-N-biphenyl-2-ylbenzimidoselenoate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 5 h / 0 - 20 °C

2: N,N-dimethyl-formamide; phosgene / dichloromethane / 5 h / 20 °C / Inert atmosphere

3: potassium tri-sec-butyl-borohydride / tetrahydrofuran / 20 °C

With phosgene; potassium tri-sec-butyl-borohydride; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane;
DOI:10.3998/ark.5550190.0013.714