1-[N-(2-chloro-5-nitro-phenyl)-benzimidoyl]3-(4-methoxy phenyl) thiourea

Base Information

Chemical Name:1-[N-(2-chloro-5-nitro-phenyl)-benzimidoyl]3-(4-methoxy phenyl) thiourea
CAS No.:1372687-96-1
Molecular Formula:C₂₁H₁₇ClN₄O₃S
Molecular Weight:440.91
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[N-(2-chloro-5-nitro-phenyl)-benzimidoyl]3-(4-methoxy phenyl) thiourea

Chemical Property:

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Technology Process of 1-[N-(2-chloro-5-nitro-phenyl)-benzimidoyl]3-(4-methoxy phenyl) thiourea

There total 3 articles about 1-[N-(2-chloro-5-nitro-phenyl)-benzimidoyl]3-(4-methoxy phenyl) thiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 205827-96-9
N-(2-chloro-5-nitro-phenyl)-benzamide

: 1372687-96-1
1-[N-(2-chloro-5-nitro-phenyl)-benzimidoyl]3-(4-methoxy phenyl) thiourea

Guidance literature:: Multi-step reaction with 3 steps

1: phosphorus pentachloride / toluene / 8 h / Reflux

2: acetone / 2 h / -5 °C

3: acetone / 24 h / 20 °C

With phosphorus pentachloride; In acetone; toluene;
DOI:10.1080/17415993.2011.629094

Reference yield:

: N-(2-chloro-5-nitro-phenyl)-benzimidoyl isothiocyanate

: 104-94-9
4-methoxy-aniline

: 1372687-96-1
1-[N-(2-chloro-5-nitro-phenyl)-benzimidoyl]3-(4-methoxy phenyl) thiourea

Guidance literature:: In acetone; at 20 ℃; for 24h;
DOI:10.1080/17415993.2011.629094

Reference yield:

: N-(2-chloro-5-nitro-phenyl)-benzimidoyl chloride

: 1372687-96-1
1-[N-(2-chloro-5-nitro-phenyl)-benzimidoyl]3-(4-methoxy phenyl) thiourea

Guidance literature:: Multi-step reaction with 2 steps

1: acetone / 2 h / -5 °C

2: acetone / 24 h / 20 °C

In acetone;
DOI:10.1080/17415993.2011.629094