C₁₂H₁₇NO₃

Base Information

Chemical Name:C₁₂H₁₇NO₃
CAS No.:1177210-64-8
Molecular Formula:C₁₂H₁₇NO₃
Molecular Weight:223.272
Hs Code.:

C<sub>12</sub>H<sub>17</sub>NO<sub>3</sub>

Synonyms:

Suppliers and Price of C₁₂H₁₇NO₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₁₇NO₃

Chemical Property:

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Technology Process of C₁₂H₁₇NO₃

There total 6 articles about C₁₂H₁₇NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-10-7
4-dimethylamino-benzaldehyde

: 1177210-64-8
C₁₂H₁₇NO₃

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydride / methanol; diethyl ether / 18 h / 0 - 20 °C

2: hydrogenchloride / water / 0.5 h / 20 °C

3: triethylamine / dichloromethane / 16 h / 0 - 20 °C

4: hydrogen; Rh(I) [(R,R)-Dipamp](COD) / methanol / 96 h / 50 °C / 3750.38 Torr / Inert atmosphere

5: lithium hydroxide / water; tetrahydrofuran

6: thionyl chloride

With hydrogenchloride; thionyl chloride; Rh(I) [(R,R)-Dipamp](COD); hydrogen; sodium hydride; triethylamine; lithium hydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water;
DOI:10.1002/ejoc.201201506

Reference yield:

: 1431505-76-8
(R)-methyl 3-(4-dimethylaminophenyl)-2-(pivaloyloxy)propanoate

: 1177210-64-8
C₁₂H₁₇NO₃

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide / water; tetrahydrofuran

2: thionyl chloride

With thionyl chloride; lithium hydroxide; In tetrahydrofuran; water;
DOI:10.1002/ejoc.201201506

Reference yield:

: 1431505-70-2
methyl 3-(4-dimethylaminophenyl)-2-hydroxyacrylate

: 1177210-64-8
C₁₂H₁₇NO₃

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 16 h / 0 - 20 °C

2: hydrogen; Rh(I) [(R,R)-Dipamp](COD) / methanol / 96 h / 50 °C / 3750.38 Torr / Inert atmosphere

3: lithium hydroxide / water; tetrahydrofuran

4: thionyl chloride

With thionyl chloride; Rh(I) [(R,R)-Dipamp](COD); hydrogen; triethylamine; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1002/ejoc.201201506