Cu(((CH₃)3C₆H₂)2C₆H₃NC)2Cl

Base Information

• Chemical Name: Cu(((CH₃)3C₆H₂)2C₆H₃NC)2Cl
• CAS No.: 1064078-50-7
• Molecular Formula: C₅₀H₅₀ClCuN₂
• Molecular Weight: 777.959

Synonyms:

Chemical Property of Cu(((CH₃)3C₆H₂)2C₆H₃NC)2Cl

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Technology Process of Cu(((CH₃)3C₆H₂)2C₆H₃NC)2Cl

There total 3 articles about Cu(((CH₃)3C₆H₂)2C₆H₃NC)2Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.8%

2,6-bis(2,4,6-trimethylphenyl)phenyl isocyanide (1064078-46-1) + copper(l) chloride → Cu(((CH3)3C6H2)2C6H3NC)2Cl (1064078-50-7)

Guidance literature:

In dichloromethane; under N2 atm. to soln. CuCl in CH2Cl2 was added soln. excess ligand in CH2Cl2, mixt. was stirred for 1 h; mixt. was evapd. under vac., residue was dissolved in CH2Cl2, filtered, kept at -35°C for 36 h, ppt. was collected, dried in vac.; elem. anal.;

DOI:10.1021/ic8010986

Reference yield:

Cu(((CH3)3C6H2)2C6H3NC)3((CH2)4O)(1+)*CF3SO3(1-)=Cu(((CH3)3C6H2)2C6H3NC)3((CH2)4O)CF3SO3 (1064078-53-0) + tetrabutyl-ammonium chloride (1112-67-0) → Cu(((CH3)3C6H2)2C6H3NC)2Cl (1064078-50-7)

Guidance literature:

In tetrahydrofuran; under N2 atm. to soln. Bu4NCl in THF was added soln. Cu complex in THF, mixt. was stirred overnight; mixt. was evapd. under vac., residue was subjected 2 cycle slurrying in n-pentane, evapd, mixt. was stirred for 2 h in C6D6, filtered, monitoring by NMR spectroscopy;

DOI:10.1021/ic8010986

Reference yield:

Cu(((CH3)3C6H2)2C6H3NC)3((CH2)4O)(1+)*CF3SO3(1-)=Cu(((CH3)3C6H2)2C6H3NC)3((CH2)4O)CF3SO3 (1064078-53-0) + lithium chloride → Cu(((CH3)3C6H2)2C6H3NC)2Cl (1064078-50-7)

Guidance literature:

In tetrahydrofuran; under N2 atm. to slurry LiCl in THF was added soln. Cu complex in THF, mixt. was stirred overnight; mixt. was evapd. under vac., residue was subjected 2 cycle slurrying in Et2O, evapd, mixt. was stirred for 2 h in C6D6, filtered, monitoring by NMR spectroscopy;

DOI:10.1021/ic8010986

upstream raw materials:

Cu(((CH₃)3C₆H₂)2C₆H₃NC)3((CH₂)4O)⁽¹⁺⁾*CF₃SO₃^(1-)=Cu(((CH₃)3C₆H₂)2C₆H₃NC)3((CH₂)4O)CF₃SO₃

tetrabutyl-ammonium chloride

2,6-bis(2,4,6-trimethylphenyl)phenyl isocyanide

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