bis(ethyltriphenylphosphonium) bis(dithiooxalato-S,S')cuprate(II)

Base Information

Chemical Name:bis(ethyltriphenylphosphonium) bis(dithiooxalato-S,S')cuprate(II)
CAS No.:88326-20-9
Molecular Formula:C₄CuO₄S₄*2C₂₀H₂₀P
Molecular Weight:886.557
Hs Code.:

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Chemical Property of bis(ethyltriphenylphosphonium) bis(dithiooxalato-S,S')cuprate(II)

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Technology Process of bis(ethyltriphenylphosphonium) bis(dithiooxalato-S,S')cuprate(II)

There total 1 articles about bis(ethyltriphenylphosphonium) bis(dithiooxalato-S,S')cuprate(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: copper(II) choride dihydrate

: 896-33-3
ethyltriphenylphosphonium chloride

: 17148-97-9,20267-56-5
potassium 1,2-dithiooxalate

: 88326-20-9
bis(ethyltriphenylphosphonium) bis(dithiooxalato-S,S')cuprate(II)

Guidance literature:: In water; aq. soln. of C2H5(C6H5)3PCl and CuCl2*2H2O (2:1 molar ratio) was added to equivalent amount of aq. soln. of K2S2C2O2 with stirring; pptd., filtered, allowed to dry in vac., dissolved in DMF, Et2O was added, cooled to ca. -10°C, allowed to stand for ca. 4h;
DOI:10.1021/ja00316a028

Reference yield:

: 121714-78-1,24290-40-2,58694-80-7,10025-77-1,64333-00-2
iron(III) chloride hexahydrate

: 88326-20-9
bis(ethyltriphenylphosphonium) bis(dithiooxalato-S,S')cuprate(II)

: 88326-24-3
ethyltriphenylphosphonium bis(dithiooxalato-S,S')cuprate(II)

Guidance literature:: In dichloromethane; acetone; in the dark, stirred for 5 min; extd. with H2O, CH2Cl2 soln. was dried on CaSO4, pentane was added, filtered, 3:1 pentane/diethyl ether mixture was added to filtrate, was allowed to stand in dark;
DOI:10.1021/ja00316a028