Technology Process of C10H9BrN2O2S
There total 5 articles about C10H9BrN2O2S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C13H15BrN2O4S;
With
sodium tert-pentoxide;
In
methanol;
at 20 ℃;
Reflux;
Inert atmosphere;
With
potassium hydrogensulfate;
In
water;
DOI:10.1021/ml3000935
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / -78 - -20 °C / Inert atmosphere
1.2: 1.33 h / -78 °C / Inert atmosphere
2.1: N-chloro-succinimide / acetonitrile / 0.25 h / 0 °C / Inert atmosphere
2.2: 20 °C / Inert atmosphere
3.1: sodium tert-pentoxide / methanol / 20 °C / Reflux; Inert atmosphere
With
N-chloro-succinimide; n-butyllithium; sodium tert-pentoxide;
In
tetrahydrofuran; methanol; hexane; acetonitrile;
DOI:10.1021/ml3000935
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydrogencarbonate; sodium sulfite / tetrahydrofuran; water / 1 h / 75 °C / Inert atmosphere
2.1: thionyl chloride / dichloromethane / 3.5 h / 0 - 20 °C / Inert atmosphere
3.1: n-butyllithium / tetrahydrofuran; hexane / -78 - -20 °C / Inert atmosphere
3.2: 1.33 h / -78 °C / Inert atmosphere
4.1: N-chloro-succinimide / acetonitrile / 0.25 h / 0 °C / Inert atmosphere
4.2: 20 °C / Inert atmosphere
5.1: sodium tert-pentoxide / methanol / 20 °C / Reflux; Inert atmosphere
With
N-chloro-succinimide; n-butyllithium; thionyl chloride; sodium tert-pentoxide; sodium hydrogencarbonate; sodium sulfite;
In
tetrahydrofuran; methanol; hexane; dichloromethane; water; acetonitrile;
DOI:10.1021/ml3000935
