[1-(4-nitrobenzyl)quinolinium][Ni(2-thioxo-1,3-dithiole-4,5-dithiolate)2] C6NiS10(1-)*C16H13N2O2(1+), α, high temperature

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Chemical Name:[1-(4-nitrobenzyl)quinolinium][Ni(2-thioxo-1,3-dithiole-4,5-dithiolate)2] C6NiS10(1-)*C16H13N2O2(1+), α, high temperature
CAS No.:1190623-88-1
Molecular Formula:C₆NiS₁₀*C₁₆H₁₃N₂O₂
Molecular Weight:716.707
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Chemical Property of [1-(4-nitrobenzyl)quinolinium][Ni(2-thioxo-1,3-dithiole-4,5-dithiolate)2] C6NiS10(1-)*C16H13N2O2(1+), α, high temperature

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Technology Process of [1-(4-nitrobenzyl)quinolinium][Ni(2-thioxo-1,3-dithiole-4,5-dithiolate)2] C6NiS10(1-)*C16H13N2O2(1+), α, high temperature

There total 2 articles about [1-(4-nitrobenzyl)quinolinium][Ni(2-thioxo-1,3-dithiole-4,5-dithiolate)2] C6NiS10(1-)*C16H13N2O2(1+), α, high temperature which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: nickel(II) chloride hexahydrate

: 54995-25-4
4,5-bis(benzylthio)-1,3-dithiole-2-thione

: 1-(4-nitrobenzyl)quinolinium chloride

: 1190623-88-1
[1-(4-nitrobenzyl)quinolinium][Ni(2-thioxo-1,3-dithiole-4,5-dithiolate)2] C6NiS10(1-)*C16H13N2O2(1+), α, high temperature

Guidance literature:: With Na; I₂; In methanol; addn. of sodium to suspn. of dithiol deriv. in dry methanol at room temp. under N2, addn. of nickel compd., stirring for 20 min, addn. of iodineand then quinoline deriv. in methanol; filtration, evapn. of dilute acetone soln. at room temp. for 1-2 wks or evapn. of acetone/isopropanol or CH3CN/isopropanol or CH3CN solns., isolation of crystals, elem. anal.;
DOI:10.1021/ic900090e