[1-(4-nitrobenzyl)quinolinium][Ni(2-thioxo-1,3-dithiole-4,5-dithiolate)2]acetone C3H6OC6NiS10(1-)*C16H13N2O2(1+), α, high temperature, triclinic

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Chemical Name:[1-(4-nitrobenzyl)quinolinium][Ni(2-thioxo-1,3-dithiole-4,5-dithiolate)2]*acetone C3H6O*C6NiS10(1-)*C16H13N2O2(1+), α, high temperature, triclinic
CAS No.:1190623-89-2
Molecular Formula:C₃H₆O*C₆NiS₁₀*C₁₆H₁₃N₂O₂
Molecular Weight:774.787
Hs Code.:

[1-(4-nitrobenzyl)quinolinium][Ni(2-thioxo-1,3-dithiole-4,5-dithiolate)2]*acetone C3H6O*C6NiS10(1-)*C16H13N2O2(1+), α, high temperature, triclinic

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Chemical Property of [1-(4-nitrobenzyl)quinolinium][Ni(2-thioxo-1,3-dithiole-4,5-dithiolate)2]*acetone C3H6O*C6NiS10(1-)*C16H13N2O2(1+), α, high temperature, triclinic

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Technology Process of [1-(4-nitrobenzyl)quinolinium][Ni(2-thioxo-1,3-dithiole-4,5-dithiolate)2]*acetone C3H6O*C6NiS10(1-)*C16H13N2O2(1+), α, high temperature, triclinic

There total 2 articles about [1-(4-nitrobenzyl)quinolinium][Ni(2-thioxo-1,3-dithiole-4,5-dithiolate)2]*acetone C3H6O*C6NiS10(1-)*C16H13N2O2(1+), α, high temperature, triclinic which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: nickel(II) chloride hexahydrate

: 54995-25-4
4,5-bis(benzylthio)-1,3-dithiole-2-thione

: 1-(4-nitrobenzyl)quinolinium chloride

: 67-64-1
acetone

: 1190623-89-2
[1-(4-nitrobenzyl)quinolinium][Ni(2-thioxo-1,3-dithiole-4,5-dithiolate)2]*acetone C3H6O*C6NiS10(1-)*C16H13N2O2(1+), β, monoclinic

Guidance literature:: With Na; I₂; In methanol; addn. of sodium to suspn. of dithiol deriv. in dry methanol at room temp. under N2, addn. of nickel compd., stirring for 20 min, addn. of iodineand then quinoline deriv. in methanol; filtration, quick evapn. of satd. acetone soln., isolation of crystals, elem. anal.;
DOI:10.1021/ic900090e

Reference yield:

: nickel(II) chloride hexahydrate

: 54995-25-4
4,5-bis(benzylthio)-1,3-dithiole-2-thione

: 1-(4-nitrobenzyl)quinolinium chloride

: 67-64-1
acetone

: 1190623-89-2
[1-(4-nitrobenzyl)quinolinium][Ni(2-thioxo-1,3-dithiole-4,5-dithiolate)2]*acetone C3H6O*C6NiS10(1-)*C16H13N2O2(1+), α, high temperature, triclinic

Guidance literature:: With Na; I₂; In methanol; addn. of sodium to suspn. of dithiol deriv. in dry methanol at room temp. under N2, addn. of nickel compd., stirring for 20 min, addn. of iodineand then quinoline deriv. in methanol; filtration, evapn. of satd. acetone soln. at room temp. for 1-2 wks, isolation of crystals, elem. anal.;
DOI:10.1021/ic900090e