C₂₈H₄₄O₄Si

Base Information

• Chemical Name: C₂₈H₄₄O₄Si
• CAS No.: 1450835-72-9
• Molecular Formula: C₂₈H₄₄O₄Si
• Molecular Weight: 472.74
• Mol file: 1450835-72-9.mol

Synonyms:

Chemical Property of C₂₈H₄₄O₄Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₈H₄₄O₄Si

There total 2 articles about C₂₈H₄₄O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2-Methoxyethoxymethyl chloride (3970-21-6) + C24H36O2Si (1450835-70-7) → C28H44O4Si (1450835-72-9)

Guidance literature:

In dichloromethane;

DOI:10.1055/s-0033-1339172

Reference yield:

oct-1-ene (111-66-0,25068-25-1) → C28H44O4Si (1450835-72-9)

Guidance literature:

Multi-step reaction with 3 steps

1: AD-mix β / tert-butyl alcohol; water

2: N,N-dimethyl-formamide

3: dichloromethane

With AD-mix β; In dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 1: |Sharpless Asymmetric Epoxidation;

DOI:10.1055/s-0033-1339172

Reference yield:

C28H44O4Si (1450835-72-9) → mniopetal C (158761-00-3)

Guidance literature:

Multi-step reaction with 5 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran

2: Dess-Martin periodane / dichloromethane

3: sodium chlorite / tert-butyl alcohol

4: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C

5: zinc dibromide / dichloromethane

With dmap; sodium chlorite; tetrabutyl ammonium fluoride; Dess-Martin periodane; dicyclohexyl-carbodiimide; zinc dibromide; In tetrahydrofuran; dichloromethane; tert-butyl alcohol; 4: |Steglich Esterification;

DOI:10.1055/s-0033-1339172

upstream raw materials:

oct-1-ene

2-Methoxyethoxymethyl chloride

C₂₄H₃₆O₂Si

Downstream raw materials:

mniopetal C