C₂₀H₂₃N₃O₂S

Base Information

Chemical Name:C₂₀H₂₃N₃O₂S
CAS No.:1256261-48-9
Molecular Formula:C₂₀H₂₃N₃O₂S
Molecular Weight:369.488
Hs Code.:

C<sub>20</sub>H<sub>23</sub>N<sub>3</sub>O<sub>2</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₀H₂₃N₃O₂S

Chemical Property:

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Technology Process of C₂₀H₂₃N₃O₂S

There total 11 articles about C₂₀H₂₃N₃O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 1256261-48-9
C₂₀H₂₃N₃O₂S

Guidance literature:: Multi-step reaction with 8 steps

1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

2: iron(III) chloride hexahydrate; pyrographite; hydrazine hydrate / ethanol / Reflux

3: pyridine / chloroform / 3.5 h / 10 °C / Reflux

4: sulfuric acid; nitric acid / chloroform / 4 h / 5 °C

5: iron; acetic acid / Reflux

6: hydrogenchloride; water; acetic acid / 80 °C

7: methanol; water / 20 °C

8: sodium perborate tetrahydrate; acetic acid / 50 °C

With pyridine; hydrogenchloride; sodium perborate tetrahydrate; iron(III) chloride hexahydrate; sulfuric acid; water; nitric acid; iron; potassium carbonate; pyrographite; hydrazine hydrate; acetic acid; In methanol; ethanol; chloroform; water; N,N-dimethyl-formamide; 7: Mannich reaction;
DOI:10.1016/j.cclet.2010.05.011

Reference yield:

: C₂₀H₂₃N₃OS

: 1256261-48-9
C₂₀H₂₃N₃O₂S

Guidance literature:: With sodium perborate tetrahydrate; acetic acid; at 50 ℃;
DOI:10.1016/j.cclet.2010.05.011

Reference yield:

: 1256261-69-4
C₁₅H₁₄N₂OS

: 1256261-48-9
C₂₀H₂₃N₃O₂S

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; water / 20 °C

2: sodium perborate tetrahydrate; acetic acid / 50 °C

With sodium perborate tetrahydrate; acetic acid; In methanol; water; 1: Mannich reaction;
DOI:10.1016/j.cclet.2010.05.011