FeRu(CO)6(σ-N,μ2-N`,η2-C=N`-1,4-di-p-tolyl-1,4-diaza-1,3-butadiene)

Base Information

Chemical Name:FeRu(CO)6(σ-N,μ2-N`,η2-C=N`-1,4-di-p-tolyl-1,4-diaza-1,3-butadiene)
CAS No.:117341-41-0
Molecular Formula:C₂₂H₁₆FeN₂O₆Ru
Molecular Weight:561.296
Hs Code.:

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Chemical Property of FeRu(CO)6(σ-N,μ2-N`,η2-C=N`-1,4-di-p-tolyl-1,4-diaza-1,3-butadiene)

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Technology Process of FeRu(CO)6(σ-N,μ2-N`,η2-C=N`-1,4-di-p-tolyl-1,4-diaza-1,3-butadiene)

There total 1 articles about FeRu(CO)6(σ-N,μ2-N`,η2-C=N`-1,4-di-p-tolyl-1,4-diaza-1,3-butadiene) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 15243-33-1
dodecacarbonyl-triangulo-triruthenium

: 92218-45-6,86665-08-9,81642-76-4
Fe(CO)3(σ,σ-N,N`-1,4-di-p-tolyl-1,4-diaza-1,3-butadiene)

: 117341-41-0
FeRu(CO)6(σ-N,μ2-N`,η2-C=N`-1,4-di-p-tolyl-1,4-diaza-1,3-butadiene)

Guidance literature:: In n-heptane; refluxing under N2 for 4 h;; cooled to room temp.; filtered; evapd.; dissolved in CH2Cl2; chromd. (silcagel, hexane, then hexane/Et2O 10/1); evapd.; crystd. from hexane at -20°C; elem. anal.;;
DOI:10.1016/S0020-1693(00)86068-5

Reference yield: 35.0%

: 117341-41-0
FeRu(CO)6(σ-N,μ2-N`,η2-C=N`-1,4-di-p-tolyl-1,4-diaza-1,3-butadiene)

: 463-49-0
1,2-propanediene

: FeRu(CO)5(σ,σ-N,N`-1,4-di-p-tolyl-1,4-diaza-1,3-butadiene)(C3H4)

Guidance literature:: In hexane; a slow stream of allene was passed through a soln. of FeRu-complex at 40°C under N2;; evapd.; dissolved in CH2Cl2; chromd. (silicagel, hexane/Et2O 2/1); evapd., crystd. from hexane at -20°C; elem. anal.;;
DOI:10.1016/S0020-1693(00)86068-5