Technology Process of C13H16BrF2NO2
There total 4 articles about C13H16BrF2NO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: thionyl chloride / tetrahydrofuran
2: triethylamine / dimethyl sulfoxide
3: borane-THF / tetrahydrofuran
4: sodium hydroxide / tetrahydrofuran; water
With
thionyl chloride; borane-THF; triethylamine; sodium hydroxide;
In
tetrahydrofuran; water; dimethyl sulfoxide;
DOI:10.1016/j.bmcl.2012.08.031
- Guidance literature:
-
Multi-step reaction with 2 steps
1: borane-THF / tetrahydrofuran
2: sodium hydroxide / tetrahydrofuran; water
With
borane-THF; sodium hydroxide;
In
tetrahydrofuran; water;
DOI:10.1016/j.bmcl.2012.08.031
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium tetrahydroborate / tetrahydrofuran
2: thionyl chloride / tetrahydrofuran
3: triethylamine / dimethyl sulfoxide
4: borane-THF / tetrahydrofuran
5: sodium hydroxide / tetrahydrofuran; water
With
sodium tetrahydroborate; thionyl chloride; borane-THF; triethylamine; sodium hydroxide;
In
tetrahydrofuran; water; dimethyl sulfoxide;
DOI:10.1016/j.bmcl.2012.08.031