Technology Process of N-(2-bromo-6-phenylbenzyl)benzamide
There total 8 articles about N-(2-bromo-6-phenylbenzyl)benzamide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium carbonate;
In
dichloromethane;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 1.) tetrakis(triphenylphosphine)palladium(0), 2.) sodium carbonate / 1.) 1,2-dimethoxyethane, 20 min, 2.) 1,2-dimethoxyethane, water, reflux
2: 100 percent / hydrogen / Pd/C / ethanol / 1810.02 Torr
4: 99 percent / N-bromosuccinimide, benzoyl peroxide / CCl4 / 2 h / Heating
5: 80 percent / dimethylformamide / Ambient temperature
6: 92 percent / hydrazine hydrate / methanol / 1 h / Heating
7: 73 percent / sodium carbonate / CH2Cl2 / Ambient temperature
With
N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium(0); Perbenzoic acid; hydrogen; sodium carbonate; hydrazine hydrate;
palladium on activated charcoal;
In
methanol; tetrachloromethane; ethanol; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 100 percent / hydrogen / Pd/C / ethanol / 1810.02 Torr
3: 99 percent / N-bromosuccinimide, benzoyl peroxide / CCl4 / 2 h / Heating
4: 80 percent / dimethylformamide / Ambient temperature
5: 92 percent / hydrazine hydrate / methanol / 1 h / Heating
6: 73 percent / sodium carbonate / CH2Cl2 / Ambient temperature
With
N-Bromosuccinimide; Perbenzoic acid; hydrogen; sodium carbonate; hydrazine hydrate;
palladium on activated charcoal;
In
methanol; tetrachloromethane; ethanol; dichloromethane; N,N-dimethyl-formamide;