(S)-N-serine methylester

Base Information

• Chemical Name: (S)-N-serine methylester
• CAS No.: 155225-23-3
• Molecular Formula: C₁₅H₂₀N₂O₆
• Molecular Weight: 324.334

Synonyms:

Chemical Property of (S)-N-serine methylester

Chemical Property:

Purity/Quality:

98%,99%, ^*data from raw suppliers

CARBOBENZYLOXYSARCOSYLSERINE METHYL ESTER AldrichCPR ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (S)-N-serine methylester

There total 2 articles about (S)-N-serine methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl (2S)-2-amino-3-hydroxypropanoate hydrochloride (5680-80-8) + C14H17NO6 → (S)-N-serine methylester (155225-23-3)

Guidance literature:

With 4-methyl-morpholine; In ethyl acetate; at -15 - 20 ℃; for 13h; Yield given;

DOI:10.1016/S0957-4166(00)80107-X

Reference yield:

N-(Benzyloxycarbonyl)sarcosine (39608-31-6) → (S)-N-serine methylester (155225-23-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 4-methylmorpholine / ethyl acetate / 0.25 h / -15 °C

2: 4-methylmorpholine / ethyl acetate / 13 h / -15 - 20 °C

With 4-methyl-morpholine; In ethyl acetate;

DOI:10.1016/S0957-4166(00)80107-X

Reference yield: 85.0%

(S)-N-serine methylester (155225-23-3) → (S)-2-hydroxymethyl-4-methyl-3,6-diketopiperazine (155225-26-6)

Guidance literature:

With cyclohexene; palladium on activated charcoal; In methanol; Heating;

DOI:10.1016/j.tet.2005.06.084

upstream raw materials:

methyl (2S)-2-amino-3-hydroxypropanoate hydrochloride

N-(Benzyloxycarbonyl)sarcosine

Downstream raw materials:

(S)-2-hydroxymethyl-4-methyl-3,6-diketopiperazine

3-hydroxymethyl-4-(p-methoxybenzyl)-1-methylpiperazine-2,5-dione

(S)-3-(t-butyldimethylsilanyloxymethyl)-4-(p-methoxybenzyl)-1-methylpiperazine-2,5-dione

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