C₂₄H₄₀N₂O₅Si

Base Information

Chemical Name:C₂₄H₄₀N₂O₅Si
CAS No.:1567326-29-7
Molecular Formula:C₂₄H₄₀N₂O₅Si
Molecular Weight:464.678
Hs Code.:

C<sub>24</sub>H<sub>40</sub>N<sub>2</sub>O<sub>5</sub>Si

Synonyms:

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Chemical Property of C₂₄H₄₀N₂O₅Si

Chemical Property:

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Technology Process of C₂₄H₄₀N₂O₅Si

There total 10 articles about C₂₄H₄₀N₂O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 530-26-7
D-Mannose

: 1567326-29-7
C₂₄H₄₀N₂O₅Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: iodine / 16 h / 20 °C

2.1: sodium cyanide / water / 12 h / 50 °C

2.2: 12 h / 20 °C

3.1: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 0.25 h / -30 °C

3.2: 20 h / 20 °C

4.1: acetic acid / water / 3.5 h / 50 °C

5.1: triethylamine; dmap / dichloromethane / 12 h / 20 °C

6.1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C

7.1: triethyl phosphite / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

8.1: acetic acid; sodium cyanoborohydride / 0.5 h / 20 °C

9.1: tetrahydrofuran; methanol / 2 h / 20 °C

10.1: potassium carbonate / N,N-dimethyl-formamide

With pyridine; dmap; sodium cyanide; trifluoromethylsulfonic anhydride; iodine; sodium cyanoborohydride; potassium carbonate; Dess-Martin periodane; acetic acid; triethylamine; triethyl phosphite; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 7757-38-2,14131-84-1,23262-78-4,27108-13-0,33823-04-0,34685-42-2,57819-52-0,78039-08-4,78039-12-0,78964-16-6,94842-76-9,149342-31-4
2,3:5,6-di-O-isopropylidene-D-mannofuranose

: 1567326-29-7
C₂₄H₄₀N₂O₅Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium cyanide / water / 12 h / 50 °C

1.2: 12 h / 20 °C

2.1: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 0.25 h / -30 °C

2.2: 20 h / 20 °C

3.1: acetic acid / water / 3.5 h / 50 °C

4.1: triethylamine; dmap / dichloromethane / 12 h / 20 °C

5.1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C

6.1: triethyl phosphite / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

7.1: acetic acid; sodium cyanoborohydride / 0.5 h / 20 °C

8.1: tetrahydrofuran; methanol / 2 h / 20 °C

9.1: potassium carbonate / N,N-dimethyl-formamide

With pyridine; dmap; sodium cyanide; trifluoromethylsulfonic anhydride; sodium cyanoborohydride; potassium carbonate; Dess-Martin periodane; acetic acid; triethylamine; triethyl phosphite; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 137126-24-0
(3aR,4R,7S,7aR)-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)-7-hydroxy-2,2-dimethyltetrahydro-[1,3]-dioxolo-[4,5-c]-pyran-6-one

: 1567326-29-7
C₂₄H₄₀N₂O₅Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 0.25 h / -30 °C

1.2: 20 h / 20 °C

2.1: acetic acid / water / 3.5 h / 50 °C

3.1: triethylamine; dmap / dichloromethane / 12 h / 20 °C

4.1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C

5.1: triethyl phosphite / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

6.1: acetic acid; sodium cyanoborohydride / 0.5 h / 20 °C

7.1: tetrahydrofuran; methanol / 2 h / 20 °C

8.1: potassium carbonate / N,N-dimethyl-formamide

With pyridine; dmap; trifluoromethylsulfonic anhydride; sodium cyanoborohydride; potassium carbonate; Dess-Martin periodane; acetic acid; triethylamine; triethyl phosphite; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;