mer-(Ru(trpy)(4'-Cl-stilb)3)(PF₆)2

Base Information

Chemical Name:mer-(Ru(trpy)(4'-Cl-stilb)3)(PF₆)2
CAS No.:85680-75-7
Molecular Formula:C₅₄H₄₁Cl₃N₆Ru*2F₆P
Molecular Weight:1271.32
Hs Code.:

mer-(Ru(trpy)(4'-Cl-stilb)3)(PF<sub>6</sub>)2

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of mer-(Ru(trpy)(4'-Cl-stilb)3)(PF₆)2

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Technology Process of mer-(Ru(trpy)(4'-Cl-stilb)3)(PF₆)2

There total 1 articles about mer-(Ru(trpy)(4'-Cl-stilb)3)(PF₆)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: ammonium hexafluorophosphate

: 72905-30-7
(2,2':6',2''-terpyridine)trichlororuthenium(III)

: 2502-99-0,5847-63-2,46459-15-8,102045-66-9
(E)-4-(4-chlorostyryl)pyridine

: 85680-75-7
mer-(Ru(trpy)(4'-Cl-stilb)3)(PF₆)2

Guidance literature:: In ethanol; water; to soln. containing water, ethanol and 9-fold excess 4'-Cl-stilb added Ru(trpy)Cl3 and mixt. refluxed for 24 h, solvent volume reduced by rotary evapn., aq. NH4PF6 added; mixt. cooled, filtered and dried, residue extd. with CH2Cl2, soln. reduced, ether added, complex chromed. with 2:1 toluene/CH3CN as eluants, product isolated by repptn. from CH2Cl2 with ether, filtered and dried; elem. anal.;

Reference yield:

: 85680-75-7
mer-(Ru(trpy)(4'-Cl-stilb)3)(PF₆)2

: 85661-47-8
(Ru(trpy)(4'-Cl-stilb)3)(PF₆)2(polymer)

Guidance literature:: In acetonitrile; Electrochem. Process; electropolymerization complex in CH3CN-saturated nitrogen soln. by scanning Pt-disk potential repeatedly ca. 150 mV past E1/2 for the reductionwave of interest;