dichlorotris[benzyldiphenylphosphine]palladium(II)

Base Information

• Chemical Name: dichlorotris[benzyldiphenylphosphine]palladium(II)
• CAS No.: 1333222-00-6
• Molecular Formula: C₅₇H₅₁ClP₃Pd*Cl
• Molecular Weight: 1006.28

Synonyms:

Chemical Property of dichlorotris[benzyldiphenylphosphine]palladium(II)

Chemical Property:

Purity/Quality:

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Technology Process of dichlorotris[benzyldiphenylphosphine]palladium(II)

There total 3 articles about dichlorotris[benzyldiphenylphosphine]palladium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

sodium tetrachloropalladate(II) + benzyldiphenylphosphane (7650-91-1) → di-μ-chlorobis-[2-[(diphenylphosphino)methyl]phenyl-C,P]dipalladium(II) + dichlorotris[benzyldiphenylphosphine]palladium(II) (1333222-00-6)

Guidance literature:

With SiO₂; NaOAc; In neat (no solvent); under Ar, glove box; to PBnPh2 added Na2PdCl4, SiO2 and NaOAc, 120°C, 1 h; washed from SiO2 (acetone), solid dissolved in CH2Cl2, TLC (SiO2, CH2Cl2); elem. anal.;

DOI:10.1016/j.jorganchem.2011.06.026

Reference yield: 25.0%

sodium tetrachloropalladate(II) + benzyldiphenylphosphane (7650-91-1) → di-μ-chlorobis-[2-[(diphenylphosphino)methyl]phenyl-C,P]dipalladium(II) + trans-dichlorodi-μ-chlorobis[benzyldiphenylphosphine]dipalladium(II) (96857-75-9,96895-82-8) + dichlorotris[benzyldiphenylphosphine]palladium(II) (1333222-00-6)

Guidance literature:

With SiO₂; NaOAc; In neat (no solvent); under Ar, glove box; to PBnPh2 added Na2PdCl4, SiO2 and NaOAc, 40-120°C, 1-72 h; washed from SiO2 (acetone), solid dissolved in CH2Cl2, TLC (SiO2, CH2Cl2); elem. anal.;

DOI:10.1016/j.jorganchem.2011.06.026

Reference yield: 20.0%

sodium tetrachloropalladate(II) + benzyldiphenylphosphane (7650-91-1) → dichlorobis[benzyldiphenylphosphine]palladium(II) (61046-58-0,55529-12-9,49607-83-2) + dichlorotris[benzyldiphenylphosphine]palladium(II) (1333222-00-6)

Guidance literature:

With SiO₂; In neat (no solvent); under Ar, glove box; to PBnPh2 added Na2PdCl4, SiO2, 85°C, 5 h; washed from SiO2 (acetone), solid dissolved in CH2Cl2, TLC (SiO2, CH2Cl2); elem. anal.;

DOI:10.1016/j.jorganchem.2011.06.026

upstream raw materials:

benzyldiphenylphosphane

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