Technology Process of 3-phenyl-9H-xanthene
There total 4 articles about 3-phenyl-9H-xanthene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 150 °C
2: indium(III) triflate / di-isopropyl ether / 16 h / 80 °C / Inert atmosphere; High pressure
3: palladium diacetate; potassium carbonate; triphenylphosphine / N,N-dimethyl-formamide / 3 h / 100 °C / Inert atmosphere; Sealed tube
With
indium(III) triflate; palladium diacetate; potassium carbonate; triphenylphosphine;
In
di-isopropyl ether; N,N-dimethyl-formamide;
DOI:10.1002/cjoc.202100767
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 150 °C
2: indium(III) triflate / di-isopropyl ether / 16 h / 80 °C / Inert atmosphere; High pressure
3: palladium diacetate; potassium carbonate; triphenylphosphine / N,N-dimethyl-formamide / 3 h / 100 °C / Inert atmosphere; Sealed tube
With
indium(III) triflate; palladium diacetate; potassium carbonate; triphenylphosphine;
In
di-isopropyl ether; N,N-dimethyl-formamide;
DOI:10.1002/cjoc.202100767
- Guidance literature:
-
Multi-step reaction with 2 steps
1: indium(III) triflate / di-isopropyl ether / 16 h / 80 °C / Inert atmosphere; High pressure
2: palladium diacetate; potassium carbonate; triphenylphosphine / N,N-dimethyl-formamide / 3 h / 100 °C / Inert atmosphere; Sealed tube
With
indium(III) triflate; palladium diacetate; potassium carbonate; triphenylphosphine;
In
di-isopropyl ether; N,N-dimethyl-formamide;
DOI:10.1002/cjoc.202100767