C₁₃H₂₁NO

Base Information

Chemical Name:C₁₃H₂₁NO
CAS No.:1359985-29-7
Molecular Formula:C₁₃H₂₁NO
Molecular Weight:207.316
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₂₁NO

Chemical Property:

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Technology Process of C₁₃H₂₁NO

There total 8 articles about C₁₃H₂₁NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1202411-97-9
[(1S,3S)-3-aminocyclohexyl]methanol

: 110-13-4
2,5-hexanedione

: 1359985-29-7
C₁₃H₂₁NO

Guidance literature:: With acetic acid; In toluene; for 2h; Reflux;
DOI:10.1055/s-0031-1289884

Reference yield:

: C₁₀H₁₆O₄

: 1359985-29-7
C₁₃H₂₁NO

Guidance literature:: Multi-step reaction with 7 steps

1: diphenyl phosphoryl azide; triethylamine / toluene / 1 h / 70 °C

2: triethylamine / toluene / 5 h / 80 °C

3: lithium hydroxide monohydrate; water / tetrahydrofuran; methanol / 5 h / 20 °C

4: borane-THF / tetrahydrofuran / 4 h / -5 °C

5: Chiral Pak AD-H 250 column / ethanol; carbon dioxide / 40 °C / Resolution of racemate

6: palladium 10% on activated carbon; hydrogen / methanol / 16 h / 2585.81 Torr

7: acetic acid / toluene / 2 h / Reflux

With borane-THF; lithium hydroxide monohydrate; diphenyl phosphoryl azide; palladium 10% on activated carbon; water; hydrogen; acetic acid; triethylamine; In tetrahydrofuran; methanol; ethanol; carbon dioxide; toluene; 2: Curtius rearrangement;
DOI:10.1055/s-0031-1289884

Reference yield:

: C₁₀H₁₅N₃O₃

: 1359985-29-7
C₁₃H₂₁NO

Guidance literature:: Multi-step reaction with 6 steps

1: triethylamine / toluene / 5 h / 80 °C

2: lithium hydroxide monohydrate; water / tetrahydrofuran; methanol / 5 h / 20 °C

3: borane-THF / tetrahydrofuran / 4 h / -5 °C

4: Chiral Pak AD-H 250 column / ethanol; carbon dioxide / 40 °C / Resolution of racemate

5: palladium 10% on activated carbon; hydrogen / methanol / 16 h / 2585.81 Torr

6: acetic acid / toluene / 2 h / Reflux

With borane-THF; lithium hydroxide monohydrate; palladium 10% on activated carbon; water; hydrogen; acetic acid; triethylamine; In tetrahydrofuran; methanol; ethanol; carbon dioxide; toluene; 1: Curtius rearrangement;
DOI:10.1055/s-0031-1289884