C₃₂H₂₇NO₂

Base Information

• Chemical Name: C₃₂H₂₇NO₂
• CAS No.: 1364318-46-6
• Molecular Formula: C₃₂H₂₇NO₂
• Molecular Weight: 457.572

Synonyms:

Chemical Property of C₃₂H₂₇NO₂

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of C₃₂H₂₇NO₂

There total 1 articles about C₃₂H₂₇NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-bromo-3,5-dimethoxybenzene (20469-65-2) + N-[1,1'-biphenyl]-2-yl-[1,1'-biphenyl]-2-amine → C32H27NO2 (1364318-46-6)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; sodium t-butanolate; In toluene; for 5h; Inert atmosphere; Reflux;

DOI:10.1021/cm2020803

Reference yield:

C32H27NO2 (1364318-46-6) → C30H23NO2 (1364318-49-9)

Guidance literature:

With boron tribromide; In dichloromethane; at 20 ℃; for 48h; Inert atmosphere;

DOI:10.1021/cm2020803

Reference yield:

C32H27NO2 (1364318-46-6) → 2-[4-(N,N-bis(biphenyl-2-yl)amino)-2,6-dihydroxyphenyl]-4-[4-(N,N-bis(biphenyl-2-yl)iminio)-2,6-dihydroxycyclohexa-2,5-dien-1-ylidene]-3-oxocyclobut-1-en-1-olate

Guidance literature:

Multi-step reaction with 2 steps

1: boron tribromide / dichloromethane / 48 h / 20 °C / Inert atmosphere

2: toluene; butan-1-ol / Inert atmosphere; Reflux

With boron tribromide; In dichloromethane; toluene; butan-1-ol;

DOI:10.1021/cm2020803

upstream raw materials:

1-bromo-3,5-dimethoxybenzene

Downstream raw materials:

C₃₀H₂₃NO₂

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