Technology Process of C62H42N2O2
There total 5 articles about C62H42N2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: bromine / chloroform; acetic acid / Reflux
2: sodium t-butanolate / tris-(dibenzylideneacetone)dipalladium(0) / toluene
With
bromine; sodium t-butanolate;
tris-(dibenzylideneacetone)dipalladium(0);
In
chloroform; acetic acid; toluene;
2: Hartwig-Buchwald coupling;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / acetone / 18 h / Reflux
2: methanesulfonic acid / dichloromethane / 2 h / 5 - 20 °C
3: bromine / chloroform; acetic acid / Reflux
4: sodium t-butanolate / tris-(dibenzylideneacetone)dipalladium(0) / toluene
With
methanesulfonic acid; bromine; potassium carbonate; sodium t-butanolate;
tris-(dibenzylideneacetone)dipalladium(0);
In
dichloromethane; chloroform; acetic acid; acetone; toluene;
4: Hartwig-Buchwald coupling;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: methanesulfonic acid / dichloromethane / 2 h / 5 - 20 °C
2: bromine / chloroform; acetic acid / Reflux
3: sodium t-butanolate / tris-(dibenzylideneacetone)dipalladium(0) / toluene
With
methanesulfonic acid; bromine; sodium t-butanolate;
tris-(dibenzylideneacetone)dipalladium(0);
In
dichloromethane; chloroform; acetic acid; toluene;
3: Hartwig-Buchwald coupling;