(1R,2R)-2-nitrocyclohexyl acetate

Base Information

Chemical Name:(1R,2R)-2-nitrocyclohexyl acetate
CAS No.:1242165-55-4
Molecular Formula:C₈H₁₃NO₄
Molecular Weight:187.196
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2R)-2-nitrocyclohexyl acetate

Chemical Property:

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Technology Process of (1R,2R)-2-nitrocyclohexyl acetate

There total 3 articles about (1R,2R)-2-nitrocyclohexyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88157-64-6
trans-2-nitrocyclohexyl acetate

: 125356-60-7
(1R,2R)-2-nitrocyclohexanol

: 1242165-57-6
(1S,2S)-2-nitrocyclohexyl acetate

: 1242165-55-4
(1R,2R)-2-nitrocyclohexyl acetate

Guidance literature:: With Pseudomonas cepacia P₁ lipase; In tert-butyl methyl ether; at 20 ℃; for 24h; pH=7; optical yield given as %ee; enantioselective reaction; aq. phosphate buffer; Resolution of racemate; Enzymatic reaction;
DOI:10.1016/j.tetasy.2010.05.006

Reference yield:

: 108-05-4,9003-20-7
vinyl acetate

: 4050-48-0,43138-50-7,108267-18-1,125356-60-7,125356-64-1,125356-65-2,125409-46-3,142235-58-3
trans-2-nitro-cyclohexanol

: 125409-46-3
(1S,2S)-2-nitrocyclohexanol

: 1242165-55-4
(1R,2R)-2-nitrocyclohexyl acetate

Guidance literature:: With pseudomonas fluorescens lipase; at 20 - 40 ℃; for 27h; optical yield given as %ee; enantioselective reaction; Resolution of racemate; Enzymatic reaction;
DOI:10.1016/j.tetasy.2010.05.006

Reference yield:

: 108-05-4,9003-20-7
vinyl acetate

: 4050-48-0,43138-50-7,108267-18-1,125356-60-7,125356-64-1,125356-65-2,125409-46-3,142235-58-3
trans-2-nitro-cyclohexanol

: 125409-46-3
(1S,2S)-2-nitrocyclohexanol

: 125356-60-7
(1R,2R)-2-nitrocyclohexanol

: 1242165-55-4
(1R,2R)-2-nitrocyclohexyl acetate

Guidance literature:: With Candida cylindracea C₁ lipase; at 20 - 40 ℃; for 27h; optical yield given as %ee; enantioselective reaction; Resolution of racemate; Enzymatic reaction;
DOI:10.1016/j.tetasy.2010.05.006