Technology Process of C52H63N
There total 4 articles about C52H63N which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
ethanol; water;
for 16h;
Reflux;
DOI:10.1002/poc.2931
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: lithium hydroxide monohydrate / isopropyl alcohol / 0.33 h
1.2: 16 h / Reflux
2.1: palladium 10% on activated carbon; hydrogen / toluene / 48 h / 62059.4 Torr / Autoclave
3.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere
3.2: 16 h / -78 - 20 °C / Inert atmosphere
4.1: toluene / 16 h / Reflux
5.1: hydrogenchloride / ethanol; water / 16 h / Reflux
With
hydrogenchloride; n-butyllithium; lithium hydroxide monohydrate; palladium 10% on activated carbon; hydrogen;
In
tetrahydrofuran; ethanol; hexane; water; isopropyl alcohol; toluene;
1.1: Wittig reaction;
DOI:10.1002/poc.2931
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: lithium hydroxide monohydrate / isopropyl alcohol / 0.33 h
1.2: 16 h / Reflux
2.1: palladium 10% on activated carbon; hydrogen / toluene / 48 h / 62059.4 Torr / Autoclave
3.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere
3.2: 16 h / -78 - 20 °C / Inert atmosphere
4.1: toluene / 16 h / Reflux
5.1: hydrogenchloride / ethanol; water / 16 h / Reflux
With
hydrogenchloride; n-butyllithium; lithium hydroxide monohydrate; palladium 10% on activated carbon; hydrogen;
In
tetrahydrofuran; ethanol; hexane; water; isopropyl alcohol; toluene;
1.1: Wittig reaction;
DOI:10.1002/poc.2931
