Technology Process of C25H36O6
There total 5 articles about C25H36O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C11H24O6;
With
sodium hydride;
In
tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
at 0 - 20 ℃;
for 0.583333h;
benzyl bromide;
In
tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
at 0 - 20 ℃;
for 14.0833h;
DOI:10.1002/chem.201101437
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C / Reflux
2.1: 20% palladium hydroxide on charcoal; hydrogen / ethyl acetate / 10 h / 20 °C
3.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide; mineral oil / 0.58 h / 0 - 20 °C
3.2: 14.08 h / 0 - 20 °C
With
20% palladium hydroxide on charcoal; hydrogen; sodium hydride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/chem.201101437
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: platinum(IV) oxide; hydrogen / ethyl acetate / 1.33 h / 20 °C
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C
3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C / Reflux
4.1: 20% palladium hydroxide on charcoal; hydrogen / ethyl acetate / 10 h / 20 °C
5.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide; mineral oil / 0.58 h / 0 - 20 °C
5.2: 14.08 h / 0 - 20 °C
With
platinum(IV) oxide; lithium aluminium tetrahydride; 20% palladium hydroxide on charcoal; hydrogen; sodium hydride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/chem.201101437