2,5-dioxopyrrolidin-1-yl 21-((3aS,4S,6aR)-3-ethyl-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)-17-oxo-4,7,10,13-tetraoxa-16-azahenicosan-1-oate

Base Information

Chemical Name:2,5-dioxopyrrolidin-1-yl 21-((3aS,4S,6aR)-3-ethyl-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)-17-oxo-4,7,10,13-tetraoxa-16-azahenicosan-1-oate
CAS No.:1329611-62-2
Molecular Formula:C₂₇H₄₄N₄O₁₀S
Molecular Weight:616.733
Hs Code.:

2,5-dioxopyrrolidin-1-yl 21-((3aS,4S,6aR)-3-ethyl-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)-17-oxo-4,7,10,13-tetraoxa-16-azahenicosan-1-oate

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Chemical Property of 2,5-dioxopyrrolidin-1-yl 21-((3aS,4S,6aR)-3-ethyl-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)-17-oxo-4,7,10,13-tetraoxa-16-azahenicosan-1-oate

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Technology Process of 2,5-dioxopyrrolidin-1-yl 21-((3aS,4S,6aR)-3-ethyl-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)-17-oxo-4,7,10,13-tetraoxa-16-azahenicosan-1-oate

There total 9 articles about 2,5-dioxopyrrolidin-1-yl 21-((3aS,4S,6aR)-3-ethyl-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)-17-oxo-4,7,10,13-tetraoxa-16-azahenicosan-1-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5672-89-9
N-trifluoroacetoxy succinimide

: 1374019-73-4
C₂₃H₄₁N₃O₈S

: 1329611-62-2
2,5-dioxopyrrolidin-1-yl 21-((3aS,4S,6aR)-3-ethyl-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)-17-oxo-4,7,10,13-tetraoxa-16-azahenicosan-1-oate

Guidance literature:: With pyridine; In N,N-dimethyl-formamide;

Reference yield:

: 1374019-73-4
C₂₃H₄₁N₃O₈S

: 105832-38-0
O-(N-succinimidyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate

: 1329611-62-2
2,5-dioxopyrrolidin-1-yl 21-((3aS,4S,6aR)-3-ethyl-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)-17-oxo-4,7,10,13-tetraoxa-16-azahenicosan-1-oate

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c1cc12738a

Reference yield:

: 1374019-95-0
C₃₄H₄₀N₂O₅S

: 1329611-62-2
2,5-dioxopyrrolidin-1-yl 21-((3aS,4S,6aR)-3-ethyl-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)-17-oxo-4,7,10,13-tetraoxa-16-azahenicosan-1-oate

Guidance literature:: Multi-step reaction with 5 steps

1: water; acetic acid / 0.33 h / 20 °C

2: methanol; sodium hydroxide / 1 h / 20 °C

3: triethylamine / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

4: triethylamine / water; N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

5: triethylamine / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

With methanol; water; acetic acid; triethylamine; sodium hydroxide; In water; N,N-dimethyl-formamide;
DOI:10.1039/c1cc12738a